Method for preparing electrochemical sensor based on carbon nano tube and vinyl ferrocene modified carbon paste electrode
A vinyl ferrocene, carbon nanotube technology, applied in the direction of material electrochemical variables, can solve the problems of poor electron transfer efficiency, use of toxic organic solvents, high overpotential, achieve effective electrocatalytic activity, reduce anode overpotential Effect
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[0012] In order to deepen the understanding of the present invention, the present invention will be further described below in conjunction with implementation.
[0013] A preparation method of an electrochemical sensor based on carbon nanotubes and vinyl ferrocene modified carbon paste electrodes, the steps are as follows:
[0014] Electrode preparation: 0.01 g of vinylferrocene, 0.89 g of graphite powder and 0.1 g of carbon nanotubes were mixed in a mortar, 0.9 mL of paraffin oil was added to the mixture and mixed for 40 min until a uniform paste was formed. The paste was squeezed into the end of a glass tube with a diameter of 0.6 mm and a length of 3 cm, and a copper wire was inserted into the carbon paste as a wire.
[0015] Electrochemical measurement procedure: Electrochemical measurement is carried out on an electrochemical workstation, and a traditional three-electrode electrolytic cell is used for measurement. Ag / AgCl / KCl (1.5mol / L), platinum wire, carbon nanotubes a...
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