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Nano preservative film for preventing edible fungus from deterioration and application thereof

A technology of nano-preservation film and edible fungi is applied in the field of storage and processing of agricultural products, which can solve the problems of low material transparency, high content of silver ions, large nanoparticles, etc., and achieve the effects of improving fresh-keeping quality, high retention rate and beneficial to preservation.

Active Publication Date: 2014-11-19
灌南县金凯包装有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are still three problems to be solved in the previously developed nanomaterials: (1) In terms of appearance, due to the addition of nanoparticles and anti-fogging agents, the transparency of the previous nanomaterials is not high, which is not conducive to commercial sale; (2) In terms of microstructure, the nanoparticles are large and unevenly distributed, and agglomeration occurs in some areas; (3) In terms of safety, the silver ion content of nanomaterials was high before, and there was a certain risk of metal migration during storage

Method used

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  • Nano preservative film for preventing edible fungus from deterioration and application thereof
  • Nano preservative film for preventing edible fungus from deterioration and application thereof
  • Nano preservative film for preventing edible fungus from deterioration and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] Preparation of nano-preservative film

[0045] 1) Raw material

[0046] Nanocomposite powder mass ratio composition: nano-silver (HTB-032, Nanjing Haitai Nano Company) 30%, nano-titanium dioxide (HTTi-01, HTTi-03, Nanjing Haitai Nano Company) 35%, nano-attapulgite (HTDK , Nanjing Haitai Nano Company) 25%, nano silicon dioxide (HTSi-11, Nanjing Haitai Nano Company) 10%;

[0047] The coupling agent is silane reagent KH-570.

[0048] 2) Processing of masterbatch

[0049] Get above-mentioned nanocomposite powder 15%, low-density polyethylene (TN-26, Sinopec Qilu Petrochemical Company) 46% according to mass ratio, linear low-density polyethylene (7042, Sinopec Yangzi Petrochemical Co., Ltd.) 22%, 10% dispersant, 5% lubricant, 2% coupling agent, knead and extrude in a plasticizer (TN-26, Nanjing Keya Company, Jiangsu, China) after high-speed mixing for 0.5 hours, and cut after cooling in a cold water tank Obtain nano-masterbatch (3mm*3mm*1.5mm);

[0050] 3) Processing of...

Embodiment 2

[0057] Microstructure and physical properties of nano-preservative film

[0058] 1) Structural characterization

[0059] The complete and traceless nano-preservative film was selected to make a disc with a diameter of 1 cm. After spraying gold, the prepared sample was observed with a scanning electron microscope at an accelerating voltage of 15kV. The results show that the nano-particles of the new nano-preservation film material have a uniform particle size, between 10-50nm, and are evenly distributed, and there is no undesirable phenomenon of particle agglomeration ( figure 2 ).

[0060] 2) Determination of physical properties

[0061] According to the test method in GB 10457-2009 "Plastic self-adhesive plastic wrap for food", the physical properties of the nano-preservation film are tested. The test indicators include tensile strength, nominal strain at break, light transmittance, right-angle tear strength, and oxygen permeability. Rate, carbon dioxide permeability, moi...

Embodiment 3

[0066] Determination of Mobility of Nano-silver in Nano Preservative Film

[0067] Flammulina velutipes were packaged with nano-film and stored at 4°C and 25°C respectively. After 15 days, the silver content in mushroom body and nano-film was measured, and then the migration of nano-silver was analyzed. The results are shown in Table 2. After 15 days of storage, there was no obvious migration of silver particles in the mushroom body, and the silver content of the dry powder of the mushroom body was very low, within the safe range specified by the national standard (GB 9685-2008).

[0068] Table 2 The content of metal Ag in mushroom body (dry weight) and nanobags under different storage temperature conditions (unit: mg / kg)

[0069]

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Abstract

The invention relates to a nano preservative film for preventing edible fungus from deterioration and application thereof, and a preparation method and application thereof, belonging to the technical field of agricultural product storage processing. The preparation method comprises the following steps: taking 15 wt% of nano powder (30% of nano silver, 35% of nano titanium dioxide, 25% of nano attapulgite and 10% of nano silicon dioxide), 45 wt% of low density polyethylene, 22 wt% of low density linear polyethylene, 10 wt% of dispersing agent, 5 wt% of lubricant and 2 wt% of coupling agent, evenly mixing, extruding, cooling and carrying out set cutting to obtain a nano master batch; and taking 7.5 wt% of nano master batch, 8 wt% of antifogging agent master batch and 84.5 wt% of low density linear polyethylene, carrying out hot melt, evenly mixing, and running to form the nano preservative film with the thickness of 18 mu m. The nano preservative film is used for packaging edible fungus to form a high-humidity low-oxygen environment; the lower spoilage microorganism activity and ethylene content can effectively inhibit the after growth, deterioration and other phenomena of the edible fungus, effectively maintain the storage quality and enhance the commodity value of the edible fungus; and thus, the nano preservative film has wide market prospects.

Description

1. Technical field [0001] The invention relates to a nano-preservation film for preventing the quality deterioration of edible fungi and an application thereof, belonging to the technical field of storage and processing of agricultural products. 2. Background technology [0002] In recent years, with the transformation of food research from nutritional traditional foods to physiologically regulating functional foods, plant-based functional foods have received more and more attention. The annual output of edible fungi in my country accounts for more than 75% of the world's total output, and its total output value ranks sixth in my country's planting industry after grain, cotton, oil, vegetables, and fruits. At present, there are 70 to 80 cultivated species of edible fungi in my country, 50 species are commercialized, and more than 20 species are produced on a certain scale. Edible fungi are rich in various nutrients and functional components, and their consumption is increas...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/08C08L23/06C08K13/02C08K3/08C08K3/22C08K3/36C08K3/34C08J3/22B29C47/92B29C48/92
CPCC08K2003/2241C08L23/0815C08J3/226C08J5/18C08J2323/08C08J2423/06C08J2423/08C08K2201/011C08L2203/16C08L2205/025C08L2205/03C08L2207/066C08L23/06C08K13/02C08K2003/0806C08K3/36C08K3/34
Inventor 胡秋辉方东路杨文建赵立艳安辛欣杨方美方勇马宁刘音宏单楠陈泽徐相如
Owner 灌南县金凯包装有限公司
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