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A kind of emulsified oil for synthetic hydraulic support and preparation method thereof

A hydraulic support and emulsified oil technology, applied in the field of emulsified oil, can solve the problems of poor lubricity, affect the production of emulsified oil, stimulate the human respiratory tract, etc., reduce maintenance and use costs, solve the problem of freezing during storage and use, and have good freeze-thaw resistance sexual effect

Active Publication Date: 2018-01-16
JIANGSU XINPENG ENERGY TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing emulsified oil production mainly includes two formulations of naphthenic acid and rosin. The naphthenic acid formulation uses sodium naphthenate as the main surfactant, and sodium naphthenate is refined from petroleum (mainly naphthenic crude oil) The naphthenic acid obtained in the process is refined and then neutralized with sodium hydroxide. With the improvement and improvement of the oil refining process, the output of naphthenic acid is getting lower and lower, and the resources are seriously depleted, which has become a problem affecting the production of emulsified oil. The main obstacle; the rosin formula selects anionic rosin potassium soap as the main surfactant. Although the raw material is easy to get, the production process of rosin potassium soap is carried out by heating. In the production process, volatile organic compounds are easy to stimulate the human respiratory tract and pollute Environment, and the produced emulsified oil has poor anti-oxidation stability, darker color, and the lubricity of the emulsion is worse than that of the emulsified oil produced by sodium naphthenate

Method used

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  • A kind of emulsified oil for synthetic hydraulic support and preparation method thereof
  • A kind of emulsified oil for synthetic hydraulic support and preparation method thereof
  • A kind of emulsified oil for synthetic hydraulic support and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] An emulsified oil for a synthetic hydraulic support, consisting of the following components by weight percentage: 7 # 30% base oil, 20% sodium heavy alkylbenzene sulfonate, 10% complex of oleic acid and triethanolamine, 7% complex of alkylphenol and ethylene oxide, 4% triethanolamine, coconut oil fatty acid diethanolamide 1%, zinc naphthenate 0.6%, benzotriazole 0.2%, distilled water 27.2%.

[0018] The preparation method of the emulsified oil for the above-mentioned synthetic hydraulic support comprises the following steps:

[0019] (1) Throwing heavy alkylbenzenesulfonic acid and concentration of 18wt% sodium hydroxide solution into the reactor according to the mass ratio of 12 to 13:1 and stirring to make it fully react to uniformity, and adjust the pH value of the reaction solution to be 8 to 8. 9. The preferred pH is 8.5. After passing the inspection, put the material into the bucket after cooling to prepare sodium heavy alkylbenzene sulfonate, which is ready for ...

Embodiment 2

[0029] An emulsified oil for a synthetic hydraulic support, consisting of the following components by weight percentage: 7 # Base oil 35%, sodium heavy alkylbenzene sulfonate 22%, complex of oleic acid and triethanolamine 13%, complex of alkylphenol and ethylene oxide 5%, triethanolamine 3%, coconut oil fatty acid diethanolamide 1.5%, zinc naphthenate 0.4%, benzotriazole 0.1%, distilled water 20%.

[0030] The preparation method of the emulsified oil for the above-mentioned synthetic hydraulic support is the same as in Example 1.

[0031] After inspection, the performance parameters of the emulsified oil for synthetic hydraulic supports obtained in this example are shown in Table 2.

[0032] Table 2

[0033]

[0034]

Embodiment 3

[0036] An emulsified oil for a synthetic hydraulic support, consisting of the following components by weight percentage: 7 # Base oil 33%, sodium heavy alkylbenzene sulfonate 22%, complex of oleic acid and triethanolamine 12%, complex of alkylphenol and ethylene oxide 6%, triethanolamine 4%, coconut oil fatty acid diethanolamide 1.5%, zinc naphthenate 0.8%, benzotriazole 0.2%, distilled water 20.5%.

[0037] The preparation method of the emulsified oil for the above-mentioned synthetic hydraulic support is the same as in Example 1.

[0038] After inspection, the performance parameters of the emulsified oil for the synthetic hydraulic support obtained in this embodiment are shown in Table 3:

[0039] table 3

[0040]

[0041]

[0042] The emulsified oil produced according to the formula of the present invention has great advantages in terms of stability. Laboratory data show that it has been greatly improved in terms of thermal stability and room temperature stability. ...

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Abstract

The invention discloses an emulsified oil for a synthetic hydraulic support and a preparation method thereof. The emulsified oil is composed of the following components by weight percentage: 30% to 35% of 7# base oil, 20% to 22% of sodium heavy alkyl benzene sulfonate %, oleic acid and triethanolamine complex 10%~13%, alkylphenol and ethylene oxide complex 5%~7%, triethanolamine 3%~4%, benzotriazole 0.1%~0.2% , coconut oil fatty acid diethanolamide 1% to 1.5%, zinc naphthenate 0.4% to 0.8%, and the balance is distilled water. The method firstly synthesizes sodium heavy alkyl benzene sulfonate, the complex of oleic acid and triethanolamine, the complex of alkylphenol and ethylene oxide, and then sequentially adds the above-mentioned raw materials into the reaction kettle under normal temperature and pressure, and stirs Evenly, pass the inspection and put it into the barrel. The invention has wide selection of raw material sources, simple process, good freeze-thaw resistance, lubricity and emulsification stability, effectively reduces the problems of oil separation and soap separation, and does not block the filter screen.

Description

technical field [0001] The invention relates to an emulsified oil, in particular to an emulsified oil for a synthetic hydraulic support and a preparation method thereof. Background technique [0002] Emulsified oil for hydraulic supports is mainly used in coal mine hydraulic supports, single hydraulic props and other systems. As a power transmission medium, it needs to have good stability, rust resistance, corrosion resistance and freeze-thaw resistance, and can effectively protect the hydraulic system. , prolong its service life. The existing emulsified oil production mainly includes two formulations of naphthenic acid and rosin. The naphthenic acid formulation uses sodium naphthenate as the main surfactant, and sodium naphthenate is refined from petroleum (mainly naphthenic crude oil) The naphthenic acid obtained in the process is refined and then neutralized with sodium hydroxide. With the improvement and improvement of the oil refining process, the output of naphthenic ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10M141/08C10M161/00C10M163/00C10M167/00C10M177/00
Inventor 高静何圣龙王建和
Owner JIANGSU XINPENG ENERGY TECH