Preparation method of envelopes of phosphoric acid micropore acidulant granules
A technology of acidifier and granular material, which is applied in the field of coating preparation of feed acidifier, which can solve the problems of volatile instability, limited application, incomplete coating, etc.
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Embodiment 1
[0020] The coating preparation method of the phosphoric acid microporous acidifier granules, the specific steps are as follows:
[0021] (1) Mix 10 parts of chitosan, 10 parts of citric acid and 10 parts of malic acid through a 300-mesh sieve, add 20 parts of lactic acid and 5 parts of polyethylene glycol, mix well and then spray granulate; The temperature is 90°C, the outlet temperature is 60°C, and the granulation particle size is 100 microns.
[0022] (2) 3 parts of phosphoric acid, 1 part of formic acid, 8 parts of acetic acid, 3 parts of propionic acid, 8 parts of butyric acid, 10 parts of hydroxypropyl methylcellulose, 2 parts of fumed silicon dioxide and the preparation obtained in step (1) The granules are mixed evenly and granulated by a screw extruder; the particle size of the granulated by the screw extruder is 300 microns. During the granulation process, the left-right symmetrical high-pressure nitrogen flow with a pressure of 0.15Mpa is relatively rushed towards ...
Embodiment 2
[0026] The coating preparation method of the phosphoric acid microporous acidifier granules, the specific steps are as follows:
[0027] (1) Mix 12 parts of chitosan, 15 parts of citric acid, and 15 parts of malic acid through a 300-mesh sieve, add 30 parts of lactic acid and 8 parts of polyethylene glycol, mix well and then spray granulate; The temperature is 100°C, the outlet temperature is 70°C, and the granulation particle size is 150 microns.
[0028] (2) 5 parts of phosphoric acid, 2 parts of formic acid, 10 parts of acetic acid, 5 parts of propionic acid, 10 parts of butyric acid, 12 parts of hydroxypropyl methylcellulose, 3 parts of fumed silicon dioxide and the preparation obtained in step (1) The granules are mixed evenly and granulated by a screw extruder; the particle size of the granulated by the screw extruder is 500 microns. During the granulation process, the left-right symmetrical high-pressure argon gas flow with a pressure of 0.18Mpa is relatively rushed to...
Embodiment 3
[0032] The coating preparation method of the phosphoric acid microporous acidifier granules, the specific steps are as follows:
[0033] (1) Mix 11 parts of chitosan, 12 parts of citric acid, and 12 parts of malic acid through a 300-mesh sieve, add 25 parts of lactic acid and 7 parts of polyethylene glycol, and spray granulation after mixing evenly; The temperature is 95°C, the outlet temperature is 65°C, and the granulation particle size is 120 microns.
[0034] (2) 4 parts of phosphoric acid, 1.5 parts of formic acid, 9 parts of acetic acid, 4 parts of propionic acid, 9 parts of butyric acid, 11 parts of hydroxypropyl methylcellulose, 2.5 parts of fumed silicon dioxide and the preparation obtained in step (1) The granules are mixed evenly and granulated by a screw extruder; the particle size of the granulated by the screw extruder is 400 microns. During the granulation process, the left-right symmetrical high-pressure nitrogen flow with a pressure of 0.16Mpa is relatively r...
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