Magnetic composition and preparation method thereof
A composite composition and magnetic technology, applied in the field of magnetic composite composition and its preparation, high heat-resistant magnetic material, and high toughness, can solve the mechanical properties of composite materials, poor heat resistance, and the influence of bending head machining accuracy. Large particles, poor compatibility with organic components, etc., to achieve good bonding performance, meet development and application, and good compatibility.
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Synthetic example
[0020] Add 1000g of 2-(p-cumyl-phenoxy)-hexylacrylate and 300g of succinic anhydride to 2-hexanone, and reflux for 50 minutes; then add 500g of thioacetamide and 8.5g of imidazole, and reflux After 25 minutes, the solvent was removed by rotary evaporation to obtain an acrylic acid prepolymer.
[0021] Add 80g iron phthalocyanine and 2Kg iron ferric oxide into methanol solution containing 150g potassium hydroxylamine, stir for 1.2 hours; then add 1Kg manganese zinc ferrite powder and 160g palmitic acid in turn, stir at 60°C for 2.4 hours, then 800W Sonication for 2 minutes resulted in a filler system.
Embodiment
[0023] According to the ratio in Table 1, mix the filler system and acrylic acid prepolymer; then add 1,3,5-triglycidyl-S-triazinetrione and dibutyltin chloride to 2-hexanone in sequence, and mix well Then add ethoxylated trimethylolpropane triacrylate and linseed oil, reflux reaction for 3 hours, finally add the mixture of filler system and acrylic acid prepolymer, reflux reaction for 1 hour, volatilize and remove the solvent to obtain a magnetic composite composition .
[0024] Table 1 raw material quality / g
[0025] Example one two three Four Fives Comparative example one Comparative example two 1,3,5-Triglycidyl-S-triazinetrione 200 240 290 340 400 380 340 Dibutyltin chloride 9 9.5 10 10 9 0 2 Acrylic Prepolymer 120 114 90 97 104 100 100 Ethoxylated Trimethylolpropane Triacrylate 260 220 200 300 240 200 250 linseed oil 10 11 12 13 14 4 0 filler 100 100 100 100 100 100 100
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