Preparation method of oxide-cladding lithium ion battery positive material
An ion battery, cathode material technology, applied in battery electrodes, circuits, electrical components, etc., can solve the problem of cycle performance, poor thermal stability and high temperature performance, poor battery safety and thermal stability, difficult to achieve cobalt acid Lithium replacement and other issues, to achieve good market promotion value, good product stability, and improved cycle performance.
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Embodiment 1
[0032] (1) Preparation of manganese salt and nickel salt materials: mix manganese sulfate and nickel sulfate materials with a Mn:Ni molar ratio of 3:1;
[0033] (2) The sol-gel method prepares the nickel-manganese precursor: the mixture obtained in step (1) is added in the chelating agent polyethylene glycol-1000, and the quality of the chelating agent is 120% of the metal Mn+Ni quality, with ammonium bicarbonate Adjust the pH to 8-10, stir until viscous, add pure water under stirring to make a solution with a metal Mn+Ni ion concentration of 100g / l, add a sedimentation aid hydroxyl Methyl cellulose until the precipitation is complete, filter, and dry the precipitate to obtain a nickel-manganese precursor;
[0034] (3) Three-dimensional oblique mixing: use a three-dimensional oblique mixer to disperse and mix the nickel-manganese precursor and lithium carbonate salt obtained in step (2) for 2 hours under the medium of polyurethane balls, metal (Mn+Ni): Li moles The ratio is 0...
Embodiment 2
[0041] (1) Preparation of manganese salt and nickel salt materials: mix manganese nitrate and nickel nitrate materials with a Mn:Ni molar ratio of 3:1;
[0042] (2) The sol-gel method prepares the nickel-manganese precursor: the mixture obtained in step (1) is added in the chelating agent polyethylene glycol-4000, and the quality of the chelating agent is 100% of the metal Mn+Ni quality, with ammonium bicarbonate Adjust the pH to 8-10, stir until viscous, add pure water under stirring to make a solution with a metal Mn+Ni ion concentration of 120g / l, add a sedimentation aid hydroxyl that is 5% of the metal Mn+Ni Methyl cellulose until the precipitation is complete, filter, and dry the precipitate to obtain a nickel-manganese precursor;
[0043] (3) Three-dimensional oblique mixing: use a three-dimensional oblique mixer to disperse and mix the nickel-manganese precursor and lithium carbonate salt obtained in step (2) for 4 hours under the medium of zirconia balls, metal (Mn+Ni)...
Embodiment 3
[0050] (1) Preparation of manganese salt and nickel salt materials: mix manganese chloride and nickel chloride materials with a Mn:Ni molar ratio of 3:1;
[0051] (2) Sol-gel method to prepare nickel-manganese precursor: the mixture of step (1) gained is added chelating agent polyethylene glycol-2000, and the quality of chelating agent is 80% of metal Mn+Ni quality, adjusts with ammonium bicarbonate When the pH is 8-10, stir until viscous, add pure water under stirring to make a solution with a metal Mn+Ni ion concentration of 150g / l, and add a settling aid hydroxyformide whose mass is 4% of the mass of the metal Mn+Ni Base cellulose until the precipitation is complete, filter, and dry the precipitate to obtain the nickel-manganese precursor;
[0052] (3) Three-dimensional oblique mixing: use a three-dimensional oblique mixer to disperse and mix the nickel-manganese precursor and lithium carbonate salt obtained in step (2) for 3 hours under the medium of polyurethane balls, me...
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