Method for preparing anhydrous magnesium carbonate through magnesium-containing mother solution
A technology of anhydrous magnesium carbonate and mother liquor, applied in the direction of magnesium carbonate, chemical instruments and methods, inorganic chemistry, etc., can solve the problems of unsolved filtration, complicated process, difficult industrialization, etc., and achieve good filtration and separation performance , low process cost and simple equipment
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Embodiment 1
[0027] (1) Adjust the pH value: pass ammonia gas with a volume concentration of 95% into 1000g (volume 750mL) of magnesium-containing mother liquor magnesium sulfate subtype salt lake old brine (Mg 2+ The mass concentration is 6.5wt%), to mother liquor pH=10.56, get 765mLMg(OH) 2 slurry;
[0028] (2) CO 2 Carbonization: CO with a volume concentration of 85% 2 With the pressure of 0.1Mpa and the speed of 2.8L / L solution h, pass through the 765mLMg(OH) obtained in step (1) 2 Carry out carbonization reaction at room temperature at 20°C in the slurry, and stop the reaction when the pH value is 7.5 to obtain the carbonization mother liquor;
[0029](3) Pyrolysis separation: heat and decompose the carbonized mother liquor obtained in step (2) at 40°C for 50 minutes, and separate solid and liquid to obtain MgCO 3 ·3H 2 O solid salt and pyrolysis separation mother liquor;
[0030] (4) Calcination: MgCO obtained in step (3) 3 ·3H 2 O was calcined at 250°C for 50min to obtain 21...
Embodiment 2
[0035] (1) Adjust the pH value: pass ammonia gas with a volume concentration of 90% into 2000g (volume 1900mL) of magnesium-containing mother liquor polyhalite leaching mother liquor (Mg 2+ The mass concentration is 0.95wt%), to mother liquor pH=11.4, get 1955mLMg(OH) 2 slurry;
[0036] (2) CO 2 Carbonization: CO with a volume concentration of 95% 2 With the pressure of 0.5Mpa and the speed of 4.5L / L solution h, pass through the 1955mLMg(OH) obtained in step (1) 2 In the slurry, carry out carbonization reaction at room temperature at 30°C, and terminate the reaction when the pH value is 8.0, to obtain the carbonization mother liquor;
[0037] (3) Pyrolysis separation: heat and decompose the carbonized mother liquor obtained in step (2) at 70°C for 30 minutes, and separate solid and liquid to obtain MgCO 3 ·3H 2 O solid salt and pyrolysis separation mother liquor;
[0038] (4) Calcination: MgCO obtained in step (3) 3 ·3H 2 O was calcined at 290° C. for 40 minutes to obt...
Embodiment 3
[0043] (1) Adjust the pH value: pass ammonia gas with a volume concentration of 98% into 1500g (volume 1300mL) magnesium-containing mother liquor magnesite nitric acid leaching mother liquor (Mg 2+ The mass concentration is 2.8wt%), to mother liquor pH=11.8, get 1335mLMg(OH) 2 slurry;
[0044] (2) CO 2 Carbonization: CO with a volume concentration of 90% 2 With the pressure of 0.3Mpa and the speed of 0.7L / L solution h, pass through the 1335mLMg(OH) obtained in step (1) 2 Carry out carbonization reaction at room temperature at 25°C in the slurry, terminate the reaction when the pH value is 7.8, and obtain the carbonization mother liquor;
[0045] (3) Pyrolysis separation: heat and decompose the carbonized mother liquor obtained in step (2) at 60°C for 60 minutes, and separate solid and liquid to obtain MgCO 3 ·3H 2 O solid salt and pyrolysis separation mother liquor;
[0046] (4) Calcination: MgCO obtained in step (3) 3 ·3H 2 O was calcined at 260° C. for 60 minutes to ...
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