A particle-mixed aluminum-based self-lubricating composite material and its preparation method

A composite material and self-lubricating technology, which is applied in the field of aluminum-based self-lubricating composite materials and its preparation, can solve the problems of difficult cooling speed, poor compliance, poor embedding, and diffuse hard point damage, and achieve thermal forming , control interface response, easy-to-operate effect

Inactive Publication Date: 2017-09-05
JIANGXI UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] In the 1970s, people added solid lubricants to refractory metals such as tungsten, molybdenum, chromium, and niobium to prepare refractory metal-based self-lubricating composite materials. They are widely used in high-temperature, high-speed, and high-friction and heat-generating environments, but they are expensive. , complex molding, difficult sintering, and gradually replaced by iron-based and copper-based materials; iron-based self-lubricating composite materials have high matrix hardness, but poor corrosion resistance, easy to produce diffuse hard points, easy to produce large dual parts such as shafts damage; copper-based self-lubricating composite materials have high comprehensive performance, but poor compliance and embedding, and relatively high cost; silver-based self-lubricating composite materials have great advantages in the electronic field, nickel-based high-temperature self-lubricating composite materials Lubricating composite materials are mainly used in high temperature fields, but the cost is high
The wettability between graphite and metal melt is poor, and the cooling rate that is swallowed or captured by aluminum melt is difficult to achieve, resulting in a large amount of agglomeration at the grain boundary and resulting in microstructure segregation

Method used

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  • A particle-mixed aluminum-based self-lubricating composite material and its preparation method

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preparation example Construction

[0040] The preparation method of titanium carbide silicide+graphite hybrid aluminum-based self-lubricating composite material described in the present invention, the more detailed steps are as follows, the process flow can refer to figure 1 :

[0041] Step 1) Ti 3 SiC 2 Preprocessing of Ti 3 SiC 2 Put the particles in acetone solution for ultrasonic cleaning for 30-45min, dry in the air, heat to 500-600℃, and keep warm for 1-3h;

[0042] Step 2) Prepare 40-60vol.% Ti 3 SiC 2 / Al Prefab: Add Ti 3 SiC 2 Put the particles into the mold and keep the pressure for 20-40s under the molding pressure of 35-55MPa, and the mold and the Ti 3 SiC 2 Preheat the particles together to 510-600°C; melt pure aluminum in the atmosphere, after the melt is refined, degassed, and slag removed, the melt temperature is controlled at 680-770°C, and poured into the preheated mold. Then under the percolation pressure of 40-50MPa in vacuum condition, hold the pressure for 10-30min, demould after...

Embodiment 1

[0055] Ti 3 SiC 2 The particles were put into acetone solution for ultrasonic cleaning for 30min, dried in the air and then heated to 500°C for 1h to complete the Ti 3 SiC 2 Pretreatment process; Ti 3 SiC 2 Put the pellets into the mold and keep the pressure for 20s under the molding pressure of 35MPa, and the mold and Ti 3 SiC 2 Commonly preheated to 510°C. At the same time, pure aluminum is smelted in the atmosphere. After the melt is refined, degassed, and slag removed, the melt temperature is controlled at 680°C, poured into the preheated mold, and then 10 -3 Under the condition of Pa vacuum, the seepage pressure is 40MPa and the pressure is maintained for 10min. After cooling, the mold is demoulded to obtain 50vol.%Ti 3 SiC 2 / Al prefabricated block, complete the prefabricated block preparation process.

[0056]Put the activated graphite powder into a beaker, then add zinc powder, dilute with acetic acid, stir the graphite powder and zinc powder evenly, add the pr...

Embodiment 2

[0061] Ti 3 SiC 2 The particles were put into acetone solution for ultrasonic cleaning for 35 minutes, dried in the air and then heated to 550°C for 1.5 hours to complete the Ti 3 SiC 2 Pretreatment process; Ti 3 SiC 2 Put the pellets into the mold and keep the pressure for 30s under the molding pressure of 40MPa, the mold and Ti 3 SiC 2 Commonly preheated to 550°C. At the same time, pure aluminum is smelted in the atmosphere. After the melt is refined, degassed, and slag removed, the melt temperature is controlled at 700°C, poured into the preheated mold, and then 10 -3 Under the vacuum condition of Pa, the percolation pressure is 45MPa and the pressure is maintained for 15min. After cooling, the mold is demoulded to obtain 50vol.%Ti 3 SiC 2 / Al prefabricated block, complete the prefabricated block preparation process;

[0062] Put the activated graphite powder into a beaker, then add zinc powder, dilute with acetic acid, stir the graphite powder and zinc powder evenl...

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Abstract

The invention discloses a particle-mixed aluminum-based self-lubricating composite material and a preparation method thereof. In terms of preparation, the combination of semi-solid stirring casting and high cooling rate directional solidification is used to overcome the macroscopic inhomogeneity of particle distribution caused by the difference in density between the added particles and the matrix metal through semi-solid stirring casting, and through high cooling rate directional solidification The method alleviates the inhomogeneous distribution of grain boundaries and grains in the matrix metal caused by the difference in particle wettability. In terms of component design, graphite (lower density, poor wettability) and cermet particles Ti3SiC2 (density Larger, better wettability) two kinds of particles, which are differentiated in density and wettability from the configuration of the matrix metal, further reducing the macroscopic and microscopic inhomogeneity of the particle distribution. The prepared self-lubricating composite material has good strength, high wear resistance and good plasticity, and can realize hot forming. The preparation method of the invention is simple, easy to operate and easy to control the process.

Description

technical field [0001] The invention relates to a self-lubricating composite material and a preparation method thereof, in particular to an aluminum-based self-lubricating composite material mixed with titanium carbide silicide particles and graphite powder particles and a preparation method thereof. Background technique [0002] Self-lubricating materials are divided into three categories: polymer-based, ceramic-based and metal-based. Metal-based self-lubricating composite materials have both the characteristics of metal substrates and the tribological characteristics of solid lubricants, and are suitable for use in atmospheric environments, chemical environments, electrical environments and The use under various conditions such as high temperature and high vacuum has become a hot spot in research and development in the field of material science. [0003] In the 1970s, people added solid lubricants to refractory metals such as tungsten, molybdenum, chromium, and niobium to ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C21/14C22C21/02C22C32/00C22C1/03C22C1/10
CPCC22C1/026C22C1/03C22C1/101C22C21/02C22C21/14C22C32/0052C22C32/0084C22C1/12C22C1/1047
Inventor 张建波汪航李勇肖翔鹏陈辉明陈婷婷胡美俊刘文扬
Owner JIANGXI UNIV OF SCI & TECH
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