Preparing method of implant nanotube array with implant material surface subject to secondary anode and broaching treatment and surface hydrophilicity
A technology of nanotube arrays and implant materials, which is applied in the field of surface hydrophilicity and preparation of implant nanotube arrays. It can solve the problems of no biological activity, weak ability to induce osteogenesis, and loosening of implant dentures. Chemical stability, uniform pore size distribution, and optimized surface properties
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[0028] (1) Select pure titanium to process it into a dental implant matrix, polish it to a mirror surface in water sequentially with silicon carbide sandpaper from 400 mesh to 8000 mesh, then use acetone, absolute ethanol, and deionized water to ultrasonically clean for 10 minutes each, and then dry it. use;
[0029] (2) Electrolyte preparation: the volume fraction is 0.5% HF+99.5% deionized water;
[0030] (3) Chemical polishing: the volume fraction is (2%-8%) HF+(10%-20%) nitric acid+(72%-88%) distilled water, the polishing time is 5 minutes, absolute ethanol, deionized water ultrasonic Wash for 5 minutes each, then blow dry for later use;
[0031] (4) Primary anode: titanium implant matrix is the anode, graphite is the cathode, the DC stable voltage is 20V, the time is 1 hour, the speed of the magnetic stirrer is 350 rpm, the distance between the two poles is 8 cm, and the temperature is room temperature. Wash with absolute ethanol and deionized water, dry (see attached...
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