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A preparation method of luminous refractory fiber needle-punched fabric

A technology for refractory fibers and needle-punched fabrics, which is applied in the direction of fabric surface trimming, heating/cooling fabrics, non-woven fabrics, etc., can solve problems such as the lack of luminous refractory fiber products, and achieve the effects of low cost, bright colors and long light effect.

Active Publication Date: 2018-11-30
CHANGXING MENGYOU REFRACTORIES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the research on luminous refractory fiber products is relatively lacking, and there is no relevant literature report

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] 20.2 wt% hydroxyapatite, 21.1 wt% dolomite, 37.6 wt% basalt, 10.0 wt% wollastonite, 2.3 wt% zircon, 2.6 wt% xenotime, 2.3 wt% strontite, carbon black 2.1 wt% and titanium dioxide 1.8 wt%, its chemical composition is calcium oxide 32.2 wt%, silicon dioxide 34.7 wt%, magnesium oxide 20.5 wt%, zirconium dioxide 2.2 wt%, diyttrium trioxide 2.3 wt%, strontium oxide 2.3 wt%, carbon 3.0 wt%, titanium dioxide 2.6 wt%, blended and crushed to 150 mesh to obtain the main raw material. Weigh 52 wt% of barium sulfate, 38 wt% of magnesium sulfate, 5 wt% of zinc sulfate, 2 wt% of lithium phosphate, and 3 wt% of copper nitrate, and use a mechanical ball mill to grind to 200 mesh to obtain red luminous powder. Put the main raw material into the melting furnace and heat it to 1900°C until it is completely melted to obtain a molten liquid. Impurities in the molten liquid are then filtered, and the filtrate flows into a stirred tank at 2100° C. and continuously stirred to obtain a spinnin...

Embodiment 2

[0038] 32.1 wt% hydroxyapatite, 16.1 wt% dolomite, 21.3 wt% basalt, 17.2 wt% wollastonite, 3.1 wt% zircon, 3.2 wt% xenotime, 2.7 wt% strontite, carbon black 2.2 wt% and titanium dioxide 2.8 wt%, its chemical composition is calcium oxide 43.1 wt%, silicon dioxide 27.4 wt%, magnesium oxide 15.2 wt%, zirconium dioxide 2.9 wt%, yttrium trioxide 2.8 wt%, strontium oxide 2.7 wt%, carbon 3.1 wt%, titanium dioxide 2.9 wt%, blended and crushed to 200 mesh to obtain the main raw material powder. Weigh calcium sulfide 58wt%, sodium sulfate 5 wt%, potassium sulfate 5 wt%, sodium sulfate 5 wt%, strontium sulfate 10 wt%, sodium chloride 6 wt%, silver nitrate 1 wt%, magnesium sulfide 10 wt%, Use a mechanical ball mill to grind to 300 mesh to obtain blue luminous powder. The main raw material powder is put into a melting furnace and heated to 2000°C until it is completely melted to obtain a molten liquid. Impurities in the molten liquid are then filtered, and the filtrate flows into a stirr...

Embodiment 3

[0041] 19.3 wt% hydroxyapatite, 23.5 wt% dolomite, 32.7 wt% basalt, 8.2 wt% wollastonite, 5.1 wt% zircon, 2.9 wt% xenotime, 3.1 wt% strontite, carbon black 2.9 wt% and titanium dioxide 23 wt%, its chemical composition is calcium oxide 30.6 wt%, silicon dioxide 29.2 wt%, magnesium oxide 22.4 wt%, zirconium dioxide 4.9 wt%, yttrium trioxide 2.5 wt%, strontium oxide 3.1 wt%, carbon 4.1 wt%, titanium dioxide 3.3 wt%, blended and crushed to 175 mesh to obtain the main raw material powder. Weigh 50 wt% of calcium sulfide, 6 wt% of potassium sulfide, 7 wt% of sodium sulfide, 12 wt% of barium nitrate, 12 wt% of zinc nitrate, and 13 wt% of indium nitrate, and use a mechanical ball mill to grind to 200-300 mesh to obtain green Luminous powder. The main raw material powder is put into the melting furnace and heated to 1950°C until it is completely melted to obtain a molten liquid. Impurities in the molten liquid are then filtered, and the filtrate flows into a stirred tank at 2150° C. ...

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Abstract

The invention discloses a preparation method for a noctilucent refractory fiber needle-punched fabric. The fabric is made of calcium oxide with the mass percent of 30%-45%, silicon dioxide with the mass percentage of 25%-50%, magnesium oxide with the mass percent of 15%-25%, zirconium oxide with the mass percent of 1%-5%, yttria with the mass percent of 1%-5%, strontium oxide with the mass percent of 1%-5%, carbon with the mass percent of 1%-5%, and titanium dioxide with the mass percent of 1%-5%. According to the invention, hydroxylapatite, dolomite, basalt, aedelforsite, zircon, xenotime, strontianite, carbon black and titanium dioxide are used as the main raw materials; during centrifugal swinging, assistance of industrial nitrogen is used to adhere noctilucent powder onto the surface of a spinning solution, so that noctilucent refractory fibers are prepared; and the noctilucent needle-punched fabric can be obtained through needle punching, and pressurization thermal shaping. The noctilucent refractory fiber needle-punched fabric obtained with the method disclosed by the invention send out colored light such as red, blue, purple and green light at night or at dark places and has high biologic solubility and structural stability.

Description

technical field [0001] The invention belongs to the field of refractory fibers, and in particular relates to a method for preparing luminous refractory fiber needle-punched fabrics. Background technique [0002] Most refractory fibers are used to replace refractory bricks in high-temperature fields such as heat treatment furnaces and heating furnaces. However, since the 1990s, with the development and promotion of new products, refractory materials have gradually entered people's daily life. Patent CN1229864A discloses a non-combustible blended yarn and its application. The fabric is obtained by blending and weaving aluminum silicate ceramic refractory fiber and glass fiber or high silica fiber, and the obtained fabric has good non-combustibility. Patent CN1253645C discloses a kind of fireproof rolling shutter, takes refractory fiber blanket as curtain core, has played important effect for the fire prevention of large-scale public place, warehouse. [0003] With the improve...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D04H1/4209D04H1/46D06C7/02C04B35/057C04B35/14C04B35/622
CPCC04B35/057C04B35/14C04B35/62231C04B2235/3206C04B2235/3213C04B2235/3225C04B2235/3232C04B2235/3244C04B2235/422D04H1/4209D04H1/46D06C7/02
Inventor 佘玉明
Owner CHANGXING MENGYOU REFRACTORIES