High-heat-conduction near-net-shaped diamond/copper composite and preparing method thereof
A composite material and diamond technology, applied in the field of metal materials, can solve the problems of poor compatibility between diamond and metal, single shape of composite material, low surface quality, etc., to reduce interface thermal resistance, high surface quality, and improve two-phase compatibility. sexual effect
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Embodiment 1
[0034] 200g of diamond particles with an average particle size of 105μm are cleaned, degreased and roughened, mixed with 2380gW powder in a ball mill and taken out, under the protection of a mixed salt bath (the mass ratio of KCl and NaCl is 1:1) Heating to 1150°C, keeping it warm for 120min, and cooling with the furnace to obtain diamond particles with a W-cured surface. The thickness of the tungsten coating and the carbide layer of tungsten is 3 μm; Raw materials in terms of weight ratio: 50% paraffin wax, 20% high-density polyethylene, 10% stearic acid and 20% polypropylene) according to the mass ratio of 13:1, fully mixed to form feed, injected on the injection molding machine, degreased Finally, a porous diamond preform is obtained. Place an appropriate amount of copper on top of the diamond preform, wherein the mass ratio of copper and diamond preform is 3:1, heat to 1300°C in an argon atmosphere, keep it warm for 60min, and cool with the furnace. The resulting diamond / ...
Embodiment 2
[0036] 200g of diamond particles with an average particle size of 105μm are cleaned, degreased and roughened, mixed with 3570gW powder in a ball mill and taken out. Heating to 1150°C, keeping it warm for 120min, and cooling with the furnace to obtain diamond particles with a W-cured surface. The thickness of the tungsten coating and the carbide layer of tungsten is 3 μm; Raw materials in terms of weight ratio: 40% paraffin wax, 25% high-density polyethylene, 10% stearic acid and 25% polypropylene) according to the mass ratio of 13:1, fully mixed to form feed, injection molding on the injection molding machine, degreasing Finally, a porous diamond preform is obtained. Place an appropriate amount of copper on top of the diamond preform, wherein the mass ratio of copper and diamond preform is 4:1, heat to 1400°C in an argon atmosphere, keep it warm for 60min, and cool with the furnace. The resulting diamond / copper composite has a thermal conductivity of 498 W.m -1 .K -1 , The ...
Embodiment 3
[0038] 20g of diamond particles with an average particle size of 105μm are cleaned, degreased, and roughened, mixed with 357gW powder in a ball mill, taken out, and protected in a mixed salt bath (the mass ratio of KCl and NaCl is 1:1). Heating to 1150°C, keeping it warm for 20 minutes, and cooling with the furnace to obtain diamond particles with a surface W, the thickness of the tungsten coating and the carbide layer of tungsten is 1 μm; Raw materials by weight ratio: 60% paraffin wax, 16% high-density polyethylene, 8% stearic acid and 16% polypropylene) are fully mixed at a mass ratio of 13:1, pressed into a mold, and porous diamonds are obtained after degreasing Preform: Place an appropriate amount of copper on top of the diamond preform, where the mass ratio of copper and diamond preform is 2:1, heat it to 1300°C in an argon atmosphere, keep it warm for 60 minutes, and cool with the furnace. The resulting diamond / copper composite has a thermal conductivity of 670 W.m -1 ...
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