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A preparation method of doped single crystal multi-core optical fiber and doped single crystal multi-core optical fiber

A technology of multi-core optical fiber and holey optical fiber, which is applied in the field of optical fiber, can solve the problems that the fiber core is difficult to ensure single crystal, pollution, and cannot form single crystal, etc., and achieves the effect of simple and practical preparation process, simple manufacturing process and less crystal defects

Active Publication Date: 2019-09-27
HARBIN ENG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The disadvantages of this optical fiber preparation method are: firstly, due to the surface electrostatic attraction, it is difficult to insert long-scale micro-single crystals into the micropores of the cladding sleeve; secondly, the large difference between the softening temperature point of quartz glass and the crystal melting point leads to In the process of stretching the cladding sleeve, the volatilization of the core melt occurs discontinuously or missing, and the quartz dissolves in the core melt, resulting in impurity pollution and hindering the crystallization process of the core melt, so that no single crystal can be formed; third, The stretching temperature gradient of the cladding sleeve is much higher than the temperature gradient force that promotes the nucleation and growth of the core melt to form a single crystal, which does not meet the kinetic conditions of single crystal growth
[0005] To sum up, the above-mentioned crystal fiber either has no cladding structure, or the core is difficult to guarantee to be a single crystal, and the fiber usually only contains a pure crystal core, which does not involve ion doping, so the prepared The function of the crystal fiber is limited, and it cannot meet the needs of further optical fiber sensing and new fiber integrated devices.

Method used

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  • A preparation method of doped single crystal multi-core optical fiber and doped single crystal multi-core optical fiber
  • A preparation method of doped single crystal multi-core optical fiber and doped single crystal multi-core optical fiber
  • A preparation method of doped single crystal multi-core optical fiber and doped single crystal multi-core optical fiber

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Embodiment 1

[0041] figure 1 It is a cross-sectional schematic diagram of the first magnesium ion-doped lithium niobate single crystal double-core optical fiber of the present invention. The core 1 is a magnesium ion-doped lithium niobate single crystal, and the position of the fiber core is asymmetrically distributed, and the cladding 2 is For quartz, the refractive index of the core 1 is greater than that of the cladding 2.

[0042] Used inner and outer double crucibles in the manufacturing process of the present invention. to combine Image 6 The outer crucible 21 is made of tungsten, with a tungsten sealing cover V on it, and a high temperature resistant (1800°C) alumina fiber sealing gasket VI is filled between the two. The outer crucible sealing cover V contains a sealing nut VII, which is porous After the capillary 17 passes through the small hole 31 on the sealing nut VII and the conical hole 28 on the crucible sealing cover V, it is inserted into the melt 23 of the inner crucibl...

Embodiment 2

[0048] combine image 3 and Figure 4 , another preparation method of magnesium ion-doped lithium niobate single crystal double-core optical fiber of the present invention is, in a section of diameter Two diameters are punched on a solid quartz rod II with a length of 70mm 8 holes, and then weld a thin-walled quartz tube with the same outer diameter on one end of the quartz rod, heat and seal the other end of the porous quartz rod with an oxyhydrogen flame, forming a welded double-hole optical fiber preform, which is installed at one end of the quartz tube The inflating device is used to inflate the inside of the hole 8 to maintain a positive pressure of ~1000Pa; draw the double-hole optical fiber preform to the outer diameter at a temperature above 1900°C on the drawing tower The dual-bore capillary III, the dual-bore capillary contains two The asymmetric micropore 9, and the quartz cladding 10. All the other technological processes are identical with embodiment one. ...

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Abstract

The invention provides a doped monocrystal multi-core optical fiber and a preparation method thereof. According to the doped monocrystal multi-core optical fiber, two or more doped monocrystal fiber cores is arranged in the same silica cladded layer, and a low-refraction-index silicon dioxide quartz glass and high-refraction-index doped monocrystal form an optical fiber waveguide structure. The preparation method comprises the following steps: acquiring porous optical fiber preforming bars; drawing the porous optical fiber preforming bars to obtain porous capillary tubes; injecting doped crystal melt in micropores in the quartz capillary tubes at high temperature and under high pressure to form polycrystal fiber cores; and finally, carrying out transverse heating and enabling the fiber cores to be subjected to monocrystal treatment and the like to prepare the silica cladded doped monocrystal multi-core optical fiber. Capillary tube porous melt injection and later-period crystal growth are combined. The doped monocrystal multi-core optical fiber which grows by the method has the advantages of controllable wire diameter and length, optional number and arrangement of the fiber cores and the like. The doped monocrystal multi-core optical fiber can be used for miniature and online photon regulation and control phase modulators, optical switches, interferometers and the like.

Description

technical field [0001] The invention relates to an optical fiber, in particular to a doped single crystal multi-core optical fiber. The invention also relates to a method of manufacturing such an optical fiber. Background technique [0002] Single crystal optical fiber is also called crystal fiber or fiber crystal. It is a single crystal that grows crystal material into a fiber shape, with a diameter ranging from a few microns to hundreds of microns. It has both the functions of bulk crystals and ordinary silica fibers. Compared with bulk crystals, single crystal optical fibers have the characteristics of small size, high integration, and can be coupled with quartz optical fibers. It has the advantages of matching the lasers in the visible and non-visible bands, and can be used for the transmission of high-power lasers. It has important practical value in the field of optoelectronics. [0003] Ordinary pure single crystals have limited functions. In order to obtain the des...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03B37/012C03B37/014
Inventor 张涛辛一凡王敬轩佟成国李见奇耿涛王鹏飞苑立波
Owner HARBIN ENG UNIV
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