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Preparation method of anti-fouling composite insulator shed rubber

A composite insulator, pollution-resistant technology, applied in the direction of organic insulators, insulators, plastic/resin/wax insulators, etc., can solve the problems of limited practical application, high preparation cost, limited production scale-up, etc., to achieve the solution of adsorption pollution, excellent stability resistance, anti-icing effect

Inactive Publication Date: 2017-11-28
HEBEI SILICON VALLEY CHEM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

One is that the preparation process of complex micro-nano materials limits its production scale; the other is the combination of the surface and the substrate and certain durability; the third is that the high cost of preparation limits the practical application

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] The present invention comprises the following steps:

[0014] 1), prefabrication of superhydrophobic mixed nano-powder material: add 120 mass parts of nano-silicon dioxide, 80 mass parts of nano-titanium dioxide, 40 mass parts of nano-calcium phosphate and 60 mass parts of nano-zinc oxide in the fluidized bed reactor. Dehydration and drying at 90°C and vacuum -0.09MPa for 2 hours; 100 parts by mass of silazane and 60 parts by mass of alkylsiloxane are passed into the fluidized bed reactor in the form of air flow, and the fluidized reaction is carried out at 150°C for 3 hours, and then vacuumized- Remove volatile matter at 0.09MPa for 1 hour to obtain super-hydrophobic nano-powder material;

[0015] 2), refining of rubber materials for umbrella covers: add 80 parts by mass of fluorinated polyimide, 150 parts by mass of fluorosilicone rubber and 360 parts by mass of methylvinyl silicone rubber in the rubber mixer, and add the superhydrophobic Mix nano-powder and refine a...

Embodiment 2

[0020] The present invention comprises the following steps:

[0021] 1), prefabrication of superhydrophobic mixed nano-powder material: add 150 mass parts of nano-silicon dioxide, 100 mass parts of nano-titanium dioxide, 70 mass parts of nano-calcium phosphate and 80 mass parts of nano-zinc oxide in the fluidized bed reactor. Dehydration and drying at 100°C and vacuum -0.09MPa for 2 hours; 150 parts by mass of silazane and 100 parts by mass of alkylsiloxane are passed into the fluidized bed reactor in the form of air flow, and the fluidized reaction is carried out at 180°C for 4 hours, and then vacuumized- Remove volatile matter at 0.09MPa for 1 hour to obtain super-hydrophobic nano-powder material;

[0022] 2), rubber refining for umbrella covers: add 120 parts by mass of fluorinated polyimide, 100 parts by mass of fluorosilicone rubber and 450 parts by mass of methyl vinyl silicone rubber in the rubber mixer, add the superhydrophobic Mix nano-powder and refine at 100°C for ...

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Abstract

The invention relates to a preparation method of anti-fouling composite insulator shed rubber. The method comprises the following steps: (1) prefabricating a super-hydrophobic mixed nano powder material, namely adding nano-silica, nanometer titania, nano calcium phosphate and nano zinc oxide to a fluidized bed reactor, carrying out dewatering and drying, introducing silazane and alkyl siloxane into the fluidized bed reactor in an airflow form, carrying out fluidization reaction, vacuumizing and removing volatile matters to prepare a mixed nano powder material; and (2) refining the rubber for a shed, namely adding fluorinated polyimide, fluorinated silicone rubber and methyl vinyl silicone rubber to a rubber mixing mill, mixing and then adding the super-hydrophobic mixed nano powder for refining, adding aluminum oxide, barium oxide and zinc oxide superfine powder for refining; adding ferrocene, aluminum chloride, titanium chloride, tetrakis dimethyl amino hafnium and ammonium iodide and mixing at constant temperature; adding a peroxide vulcanization initiator, mixing at the constant temperature until an even effect is achieved; and transferring the material to a twin-screw extruder and extruding to prepare the shed rubber.

Description

technical field [0001] The invention belongs to the field of composite insulators, and in particular relates to a preparation method of a pollution-resistant composite insulator sheath rubber. Background technique [0002] With the development of the times, composite insulators have been continuously improved and improved, and the scale of using composite insulators in power grids is increasing. In my country, composite insulators have been applied to various voltage levels of high voltage, ultra-high voltage and ultra-high voltage in the power industry. The increase in mechanical loads on insulators, the diversity of operating environments, and the aggravation of air pollution have exposed the performance of composite insulators during use. Defects. Composite insulators are more polluted than porcelain insulators in dirty operating environments, which offsets the advantages of certain hydrophobicity on the surface, and even causes hydrophilic, scaling, freezing, hydrolysis,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L83/08C08L79/08C08L83/07C08K13/06C08K9/06C08K3/36C08K3/22C08K3/32C08K5/56C08K3/16C08K3/28C08J7/00H01B3/46H01B3/30H01B17/38H01B17/50
CPCC08L83/08C08J7/08C08K2003/164C08K2003/2206C08K2003/2227C08K2003/2241C08K2003/2296C08K2003/325C08K2201/011C08K2201/014C08L79/08H01B3/306H01B3/46H01B17/38H01B17/50C08L83/04C08K13/06C08K9/06C08K3/36C08K3/22C08K3/32C08K5/56C08K3/16C08K3/28
Inventor 宋志强宋福如宋利强游传榜
Owner HEBEI SILICON VALLEY CHEM CO LTD
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