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The present application relates to volatile gas treatment technical field, disclose a kind of organic liquid volatilization inhibitor and the method for inhibiting organic liquid volatilization.The organic liquid volatilization inhibitor contains hollow microsphere, surfactant, stabilizer, dispersant, coupling agent and solvent, for inhibiting organic liquid volatilization;Wherein, the density of the organic liquid volatilization inhibitor < the density of the organic liquid.The density of the organic liquid volatilization inhibitor provided by the present application is less than volatile liquid, with certain fluidity and stability, can realize the automatic covering and complete sealing to volatile organic liquid surface, effectively prevent organic liquid volatilization during storage, loading and transportation.