Preparation method of flame-retardant thermal-insulation material
A technology of flame retardant heat preservation and raw materials, which is applied in the field of preparation of flame retardant heat insulation materials, can solve problems such as poor thermal conductivity, easy aging, poor fire safety, etc., and achieve high insulation performance, good chemical corrosion resistance, and good heat preservation performance Effect
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Embodiment 1
[0013] A method for preparing a flame-retardant thermal insulation material, comprising the following steps:
[0014] Step 1. Weigh the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 40 parts of nitrile rubber, 5 parts of acrylate rubber, 2 parts of dimethyl trimethylsilylmethylphosphonate, 4 parts of aluminum oxide, benzene 4 parts of triethoxysilane, 5 parts of sodium citrate, 15 parts of vermiculite powder, 5 parts of methyl tin mercaptide, 2 parts of calcium stearate, 15 parts of magnesium oxide powder, 13 parts of nano silicon dioxide, ten parts 2 parts of dialkylbenzenesulfonate sodium salt, 30 parts of glycerin; mix according to the proportion to obtain the mixture; put the mixture into the reaction kettle and mix for 10-15min at 100-120°C, and then extrude it with a twin-screw extruder Granulating to obtain modified pellets, and then grinding the modified pellets into 200-300 mesh fine powder;
[0015] Step 2, in parts by weight, mix 80 p...
Embodiment 2
[0017] A method for preparing a flame-retardant thermal insulation material, comprising the following steps:
[0018] Step 1. In parts by weight, the following raw materials were weighed: 110 parts of polyvinyl chloride, 50 parts of nitrile rubber, 12 parts of acrylate rubber, 4 parts of dimethyl trimethylsilyl phosphonate, 8 parts of aluminum oxide, benzene 5 parts of triethoxysilane, 7 parts of sodium citrate, 20 parts of vermiculite powder, 7 parts of methyl tin mercaptide, 4 parts of calcium stearate, 25 parts of magnesium oxide powder, 16 parts of nano silicon dioxide, ten parts 7 parts of sodium dialkylbenzenesulfonate, 40 parts of glycerin; mix in proportion to obtain a mixture; put the mixture into the reaction kettle and mix for 10-15min at 100-120°C, then extrude with a twin-screw extruder Granulating to obtain modified pellets, and then grinding the modified pellets into 200-300 mesh fine powder;
[0019] Step 2, in parts by weight, mix 100 parts of phenolic resin,...
Embodiment 3
[0021] A method for preparing a flame-retardant thermal insulation material, comprising the following steps:
[0022] Step 1. Weigh the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 40 parts of nitrile rubber, 5 parts of acrylate rubber, 2 parts of dimethyl trimethylsilylmethylphosphonate, 4 parts of aluminum oxide, benzene 4 parts of triethoxysilane, 5 parts of sodium citrate, 15 parts of vermiculite powder, 5 parts of methyl tin mercaptide, 2 parts of calcium stearate, 15 parts of magnesium oxide powder, 13 parts of nano silicon dioxide, ten parts 2 parts of dialkylbenzenesulfonate sodium salt, 30 parts of glycerin; mix in proportion to obtain a mixture; put the mixture into the reaction kettle and mix at 110°C for 13 minutes, then extrude and granulate with a twin-screw extruder to obtain Modified pellets, and then the modified pellets are ground into 200-300 mesh fine powder;
[0023] Step 2, in parts by weight, mix 60 parts of phenolic resi...
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