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Preparation method of flame-retardant thermal-insulation material

A technology of flame retardant heat preservation and raw materials, which is applied in the field of preparation of flame retardant heat insulation materials, can solve problems such as poor thermal conductivity, easy aging, poor fire safety, etc., and achieve high insulation performance, good chemical corrosion resistance, and good heat preservation performance Effect

Inactive Publication Date: 2017-12-01
苏州仲勉装饰有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In general, inorganic thermal insulation materials, such as rock wool, mineral wool, glass wool, foam concrete, vitrified microbeads, etc., although the combustion performance reaches Class A, but the thermal conductivity is poor, the thermal insulation performance is not good, and even fails when exposed to water. It is difficult to achieve the ideal heat insulation and energy saving effect when used alone
This greatly limits the scope of application of traditional building thermal insulation materials in construction engineering.
At present, the organic insulation materials used on a large scale in my country's building energy conservation mainly include EPS (polystyrene foam), PS (extruded polystyrene foam) and PU (polyurethane foam), all of which are flammable organic insulation materials. The advantages are light weight, heat preservation, and good heat insulation; the biggest defect is poor fire safety, easy aging, and easy combustion
If these new building energy-saving materials have not been modified by the chemical structure of flame retardant and smoke reduction, if they are simply added with flame retardants, there will be serious fire hazards, leading to frequent building fire accidents, CCTV fires sounded the alarm to the whole country, Therefore, the research and large-scale popularization and application of fire-proof flame-retardant technology and fire-proof structure of flammable organic thermal insulation materials have become important issues related to people's livelihood and safety in our country.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] A method for preparing a flame-retardant thermal insulation material, comprising the following steps:

[0014] Step 1. Weigh the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 40 parts of nitrile rubber, 5 parts of acrylate rubber, 2 parts of dimethyl trimethylsilylmethylphosphonate, 4 parts of aluminum oxide, benzene 4 parts of triethoxysilane, 5 parts of sodium citrate, 15 parts of vermiculite powder, 5 parts of methyl tin mercaptide, 2 parts of calcium stearate, 15 parts of magnesium oxide powder, 13 parts of nano silicon dioxide, ten parts 2 parts of dialkylbenzenesulfonate sodium salt, 30 parts of glycerin; mix according to the proportion to obtain the mixture; put the mixture into the reaction kettle and mix for 10-15min at 100-120°C, and then extrude it with a twin-screw extruder Granulating to obtain modified pellets, and then grinding the modified pellets into 200-300 mesh fine powder;

[0015] Step 2, in parts by weight, mix 80 p...

Embodiment 2

[0017] A method for preparing a flame-retardant thermal insulation material, comprising the following steps:

[0018] Step 1. In parts by weight, the following raw materials were weighed: 110 parts of polyvinyl chloride, 50 parts of nitrile rubber, 12 parts of acrylate rubber, 4 parts of dimethyl trimethylsilyl phosphonate, 8 parts of aluminum oxide, benzene 5 parts of triethoxysilane, 7 parts of sodium citrate, 20 parts of vermiculite powder, 7 parts of methyl tin mercaptide, 4 parts of calcium stearate, 25 parts of magnesium oxide powder, 16 parts of nano silicon dioxide, ten parts 7 parts of sodium dialkylbenzenesulfonate, 40 parts of glycerin; mix in proportion to obtain a mixture; put the mixture into the reaction kettle and mix for 10-15min at 100-120°C, then extrude with a twin-screw extruder Granulating to obtain modified pellets, and then grinding the modified pellets into 200-300 mesh fine powder;

[0019] Step 2, in parts by weight, mix 100 parts of phenolic resin,...

Embodiment 3

[0021] A method for preparing a flame-retardant thermal insulation material, comprising the following steps:

[0022] Step 1. Weigh the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 40 parts of nitrile rubber, 5 parts of acrylate rubber, 2 parts of dimethyl trimethylsilylmethylphosphonate, 4 parts of aluminum oxide, benzene 4 parts of triethoxysilane, 5 parts of sodium citrate, 15 parts of vermiculite powder, 5 parts of methyl tin mercaptide, 2 parts of calcium stearate, 15 parts of magnesium oxide powder, 13 parts of nano silicon dioxide, ten parts 2 parts of dialkylbenzenesulfonate sodium salt, 30 parts of glycerin; mix in proportion to obtain a mixture; put the mixture into the reaction kettle and mix at 110°C for 13 minutes, then extrude and granulate with a twin-screw extruder to obtain Modified pellets, and then the modified pellets are ground into 200-300 mesh fine powder;

[0023] Step 2, in parts by weight, mix 60 parts of phenolic resi...

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PUM

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Abstract

The invention discloses a preparation method of a flame-retardant thermal-insulation material. The preparation method comprises the following steps: uniformly mixing all materials by proportion to obtain a mixture; adding the mixture into a reaction kettle for mixing, then adopting a double-screw extruder for extrusion and granulation to obtain modified granules, and grinding into fine powder; and uniformly mixing phenolic resin and the fine powder, putting into a stirring machine for stirring, then heating and foaming to obtain the flame-retardant thermal-insulation material. The flame-retardant thermal-insulation material prepared by the preparation method is environment-friendly and wear-resistant, is applicable to a temperature range between low temperature and high temperature, has good thermal-insulation property with the service life as long as 10 years, and is high in insulating property, good in chemical-corrosion resistance and waterproof.

Description

technical field [0001] The invention relates to a preparation method of a flame-retardant thermal insulation material. technical background [0002] Building thermal insulation is an important aspect of saving energy, improving the living environment and using functions. Building energy consumption generally accounts for 30-40% of the total energy consumption of human beings, most of which are heating and air-conditioning energy consumption, so building energy conservation is of great significance. Therefore, the Ministry of Construction of the People's Republic of China No. "Management Regulations", which stipulates that in the planning, design, construction and use of urban construction in our country, building energy conservation standards must be implemented, and building structures must be treated with thermal insulation engineering. In order to save energy consumption, thermal insulation materials are usually applied on the surface of thermal equipment to reduce ene...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L61/06C08L27/06C08L9/02C08L33/04C08K13/02C08K3/22C08K3/36C08K5/098C08K5/58C08K3/34C08K5/5419C08J9/04
CPCC08L61/06C08J9/04C08J2361/06C08J2427/06C08K2003/222C08K2003/2227C08K2201/011C08K2201/014C08L2201/02C08L2203/14C08L2205/035C08L27/06C08L9/02C08L33/04C08K13/02C08K3/22C08K3/36C08K5/098C08K5/58C08K3/34C08K5/5419
Inventor 周琴
Owner 苏州仲勉装饰有限公司