Silt hardening agent and preparation method and application method thereof
A technology of curing agent and sludge, applied in the direction of dewatering/drying/concentrating sludge treatment, etc., can solve the problems of large amount of inorganic curing material added, low curing efficiency, re-leaching, etc., to shorten the curing time, high curing efficiency, The effect of reducing moisture content
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[0032] Wherein the preparation method of biomass activated carbon is: (1) impregnating biomass raw material (corn cob, coconut shell, palm shell, peanut shell, etc.) in 3mol / L ZnCl 2(solid-to-liquid mass ratio is 1: 2.5) the activation treatment of 3 days is carried out in the solution; (2) after centrifugal concentration, adopt SK2-2-10 type high-temperature tubular resistance furnace, make activation gas with water vapor (flow rate is 20L / h), heated to 600°C at a heating rate of 40°C / min for 1h activation, and finally obtained a preparation with a specific surface area of 2400m 2 / g of biomass activated carbon.
[0033] The preparation method of reduced graphene oxide is as follows: oxidizing graphite (500 mesh, Qingdao Tianyuan Graphite Co., Ltd.) with concentrated sulfuric acid / potassium permanganate, and then ultrasonically obtaining graphite oxide. Add acetylacetone to the graphite oxide aqueous solution, reflux at 80°C for 24 hours, filter, wash with ethanol, aceton...
Embodiment 1
[0038] The sludge solidifying agent is composed of sodium polyacrylate (molecular weight 1000, particle size is 300 mesh) 1%, biomass activated carbon 2%, sodium lignosulfonate 2%, polyrotaxane 1%, reduced graphene oxide 4%, cement 50% , quicklime (280 mesh) 5%, fly ash (300 mesh) 35% made.
[0039] The preparation method of the curing agent: mix and stir each raw material in a mixer according to the above mass fraction, and stir for 30 minutes.
[0040] Subsequently, the above-mentioned curing agent was added into the sludge at a mixing ratio of 20%, and after being thoroughly mixed in a mixer, it was cured for 7 days under natural sunlight.
Embodiment 2
[0042] Sludge curing agent consists of sodium polyacrylate (molecular weight 3000, particle size is 300 mesh) 2%, biomass activated carbon 3%, sodium lignosulfonate 3%, polyrotaxane 2%, reduced graphene oxide 10%, cement 40% , 10% quicklime (280 mesh) and 30% fly ash (325 mesh).
[0043] The preparation method of the curing agent: mix and stir each raw material in a mixer according to the above mass fraction, and stir for 25 minutes.
[0044] Subsequently, the above-mentioned curing agent was added into the sludge at a blending ratio of 17%, and after being thoroughly mixed in a mixer, it was cured for 7 days under natural sunlight.
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