Glass bead modified PBT material and preparation method thereof
The technology of glass microbeads and hollow glass microbeads is applied in the field of glass microbead modified PBT material and its preparation, which can solve the problems of reduced encapsulation efficiency, difficulty in controlling the curing process of epoxy resin viscosity changes, etc., so as to improve the adhesion , Excellent interface bonding effect
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[0026] Weigh: 70 kg of PBT, 18 kg of aluminum dihydrogen phosphate, 18 kg of borax, 6 kg of potassium sodium silicate, 6 kg of zinc oxide, 10 kg of hydrogenated castor oil, 2 kg of cryolite, and 2452 kg of antioxidant;
[0027] The hydrogenated castor oil includes the following parts by weight: 10 parts of PBT, 5 parts of hollow glass beads, and 2 parts of PP-g-MAH graft compatibilizer.
[0028] Specific steps are as follows:
[0029] (1) Preparation of hydrogenated castor oil:
[0030] Mix the PBT and PP-g-MAH grafting compatibilizers evenly, and pour them into the main feed port of the twin-screw extruder; put hollow glass beads into the side feed port at the rear end of the extruder; The screw extruder extrudes strands and pellets to obtain hydrogenated castor oil, ready for use;
[0031] (2) Preparation of microcapsule curing agent:
[0032] ①. Under stirring conditions, add 0.5wt% zinc oxide aqueous solution and 0.5wt% potassium sodium silicate aqueous solution, and disperse for 40...
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