Corrosion-resistant microporous mullite lightweight refractory brick and preparation method thereof

A mullite and refractory brick technology, which is applied in the field of corrosion-resistant microporous mullite lightweight refractory bricks and its preparation, can solve the problems of increasing heat energy loss, reducing the heat insulation effect of refractory materials, and increasing energy costs.

Inactive Publication Date: 2018-04-24
HENAN HAINADE NEW MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The commonly used refractory castables are mainly Al 2 o 3 -SiO 2 However, when this type of refractory material is used in petrochemical and other industries, due to the influence of the reducing atmosphere environment, the damage of the refractory material will be aggravated, thereby reducing the service life of the material
In addition, due to the large size of pores in traditional refractory aggregates, the pore diameters are mostly at the millimeter level, so when the material is used in a high temperature environment, due to the intensification of radiation heat transfer and convective heat transfer through the gas in the pores, the refractory material will The thermal conductivity of the refractory increases, which in turn reduces the heat insulation effect of the refractory material, increases the loss of heat energy, and leads to an increase in energy costs

Method used

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  • Corrosion-resistant microporous mullite lightweight refractory brick and preparation method thereof
  • Corrosion-resistant microporous mullite lightweight refractory brick and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0028] This embodiment provides a corrosion-resistant microporous mullite lightweight refractory brick, which includes a refractory brick base and a high-temperature-resistant coating coated on the surface of the refractory brick base; wherein, the preparation raw materials for the refractory brick base include : Mullite large particles 20%, andalusite small particles 15%, metakaolin superfine powder 24%, bonded clay 10%, expanded graphite 0.5%, fly ash 15%, hollow glass microspheres 4.5%, pulp water 11 %; The raw materials of the high-temperature-resistant coating include: 65% silica airgel, 15% yttrium oxide gel, 1% potassium hexatitanate whisker, 5% nano-silicon nitride, and 14% ethanol.

[0029] Wherein, the particle size of the large mullite particle is 1 mm to 3 mm, the particle size of the small andalusite particle is 0.5 mm to 1 mm, the particle size of the metakaolin superfine powder is less than 0.043 mm, and the hollow glass microsphere The length is less than 1mm. ...

Embodiment 2

[0036] This embodiment provides a corrosion-resistant microporous mullite lightweight refractory brick, including a refractory brick base and a high-temperature-resistant coating coated on the surface of the refractory brick base; wherein, the preparation raw materials for the refractory brick base: Mo 25% large stone particles, 15% small andalusite particles, 15% superfine metakaolin powder, 5% bonded clay, 1.5% expanded graphite, 18.5% fly ash, 5% hollow glass beads, and 15% pulp water; The raw materials for the preparation of the high-temperature-resistant coating include: 70% silica airgel, 15% yttrium oxide gel, 3% potassium hexatitanate whisker, 5% nano-silicon nitride, and 7% ethanol.

[0037] The preparation method of the corrosion-resistant microporous mullite lightweight refractory brick described in this example is the same as that in Example 1. After testing, the density of the corrosion-resistant microporous mullite lightweight refractory bricks prepared in this e...

Embodiment 3

[0039] This embodiment provides a kind of corrosion-resistant microporous mullite lightweight refractory brick, its structure includes a refractory brick substrate and a high temperature resistant coating coated on the surface of the refractory brick substrate; wherein, the refractory brick substrate is obtained The raw materials include: 28.5% large mullite particles, 20% small andalusite particles, 13% metakaolin superfine powder, 7% bonded clay, 1.5% expanded graphite, 15% fly ash, 5% hollow glass beads, Pulp water 10%; the raw materials for making the high-temperature-resistant coating include: silica airgel 65%, yttrium oxide gel 17%, potassium hexatitanate whiskers 3%, nano-silicon nitride 7%, ethanol 8%.

[0040] The preparation method of the corrosion-resistant microporous mullite lightweight refractory brick described in this example is the same as that in Example 1. After testing, the corrosion-resistant microporous mullite lightweight refractory brick prepared in t...

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Abstract

The invention provides a corrosion-resistant microporous mullite light-weight refractory brick, which comprises a refractory brick base and a high-temperature resistant coating coated on the surface of the refractory brick base; wherein, the raw materials of the refractory brick base include: 20% to 30% of large tolite particles, 15% to 25% of small andalusite particles, 13% to 24% of metakaolin ultrafine powder, 5% to 10% of bound clay, 0.5% to 1.5% of expanded graphite, and fly ash 15% to 20%, hollow glass microspheres 3% to 6%, and the balance is pulp water; the raw materials of the high temperature resistant coating include: silica aerogel 65% to 70%, yttrium oxide gel 15% ~ 17%, nano silicon nitride 5% ~ 10%, potassium hexatitanate whisker 1% ~ 3%, and the balance of ethanol is ethanol. The invention also provides a preparation method of the corrosion-resistant microporous mullite light refractory brick, which has simple steps and is easy to produce automatically.

Description

technical field [0001] The invention belongs to the technical field of refractory materials, and in particular relates to a corrosion-resistant microporous mullite lightweight refractory brick and a preparation method thereof. Background technique [0002] Refractory materials are widely used in metallurgy, petrochemical, glass and other high-temperature industries due to their good corrosion resistance to high-temperature media and their thermal insulation properties. As my country's emphasis on energy saving and consumption reduction continues to increase, more research and development has been done on lightweight refractory materials with good thermal insulation effects. Unshaped refractory materials have received special attention due to their advantages of convenient construction, low production cost, and good overall structure of the lining, among which refractory castables are the most widely used. [0003] The commonly used refractory castables are mainly Al 2 o 3...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B38/08C04B35/66C04B35/185C04B35/14C04B35/80C04B41/87
CPCC04B38/08C04B35/14C04B35/185C04B35/66C04B35/80C04B41/5066C04B41/87C04B2235/3225C04B2235/3418C04B2235/3463C04B2235/349C04B2235/36C04B2235/3873C04B2235/425C04B2235/5276C04B2235/96C04B41/5045C04B41/5041C04B41/5035
Inventor 张微微计富宝吉飞虎
Owner HENAN HAINADE NEW MATERIAL CO LTD
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