Acrylate structural glue suitable for zinc alloy bonding

A technology of acrylate and structural adhesives, which is applied in the direction of non-polymer organic compound adhesives, adhesives, adhesive additives, etc., and can solve problems affecting the reliability and stability of notebook machines, poor corrosion resistance, and reduced bonding strength. Problems, to achieve the effect of smooth glue, good adhesion, and even glue mixing

Active Publication Date: 2018-06-08
YANTAI DARBOND TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, zinc alloy materials also have the disadvantages of poor stability and poor corrosion resistance. At present, most acrylic structural adhesives on the market have a significant decrease in bonding s

Method used

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  • Acrylate structural glue suitable for zinc alloy bonding
  • Acrylate structural glue suitable for zinc alloy bonding
  • Acrylate structural glue suitable for zinc alloy bonding

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026]

[0027] Wherein, the surface treatment agent consists of:

[0028] Chromium phosphate: sodium sulfate: oxalic acid = 1.6: 0.8: 1

[0029] Concrete preparation steps are:

[0030] The preparation process of component A is to clean the reactor. First add 10g of methacrylic acid, 42g of methyl methacrylate, 15g of hydroxyethyl methacrylate, 6g of 2-hydroxyethyl methacrylate phosphate, methyl methacrylate-butadiene-styrene terpolymer 38g of carboxyl-terminated nitrile rubber (CTBN) 14g, stirred at high speed for 1.5h until the material was uniform and fine paste, then added 0.8g of tetramethylthiourea, 0.5g of N,N-dimethyl-p-toluidine, 0.07g of hydroquinone, 0.09g of tetrasodium edetate, and 0.13g of surface treatment agent, stirred at high speed for 1 hour, and finally evacuated for 5 minutes to defoam, and discharged to obtain component A of the finished product. In particular, during the entire stirring process, the temperature of the material in the reactor shoul...

Embodiment 2

[0033]

[0034] Wherein, the surface treatment agent consists of:

[0035] Chromium Phosphate: Sodium Sulfate: Citric Acid = 1.8:0.7:1

[0036] Concrete preparation steps are:

[0037] The preparation process of component A is to clean the reactor. First add 8g of methacrylic acid, 38g of tetrahydrofuryl methacrylate, 20g of hydroxypropyl methacrylate, 7g of 2-hydroxyethyl methacrylate phosphate, 32g of acrylonitrile-butadiene-styrene copolymer, polybutylene Diene rubber 21g, stirred at high speed for 1.5h, until the material was uniform and fine paste, then added N,N-dihydroxyethyl-p-toluidine 1g, triphenylphosphine 0.2g, p-hydroxyanisole 0.11g, sulfur Substituted diphenylamine 0.05g, surface treatment agent 0.10g, stirred at high speed for 1 hour, and finally evacuated for 5 minutes for defoaming, and discharged to obtain component A of the finished product. In particular, during the entire stirring process, the temperature of the material in the reactor should be cont...

Embodiment 3

[0040]

[0041] Wherein, the surface treatment agent consists of:

[0042] Chromium nitrate: sodium sulfate: oxalic acid = 2.0: 1.0: 1

[0043] Concrete preparation steps are:

[0044] The preparation process of component A is to clean the reactor. First add 5g of methacrylic acid, 50g of methyl methacrylate, 14g of hydroxypropyl methacrylate, 12g of 2-hydroxyethyl methacrylate phosphate, methyl methacrylate-butadiene-styrene terpolymer 40g of compound, 14g of vinyl-terminated nitrile rubber (VTBN), stirred at high speed for 1.5h, until the material was uniform and fine paste, then added 0.6g of tetramethylthiourea, 0.7g of butyraldehyde and aniline condensate amine, p-tert 0.04g of butyl catechol, 0.12g of tetrasodium ethylenediaminetetraacetic acid, and 0.16g of surface treatment agent, stirred at high speed for 1 hour, and finally evacuated for 5 minutes to defoam, and discharged to obtain component A of the finished product. In particular, during the entire stirring ...

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PUM

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Abstract

The invention relates to acrylate structural glue suitable for zinc alloy bonding. The acrylate structural glue comprises a component A and a component B. The component A comprises methacrylic acid, an acrylic monomer, a toughening agent I, a toughening agent II, a reducing agent, a stabilizer and a surface treatment agent. The component B comprises an oxidant, epoxy resin, a plasticizer, a fillerand a pigment. The above components A and B are uniformly mixed according to a volume ratio of the component A to the component B of 10: 1 to form the acrylate structural glue. The acrylate structural glue has excellent adhesiveness to conventional materials such as an ABS plastic alloy, an electrophoretic ED layer and anodized aluminum and is especially suitable for bonding of new materials in the zinc alloy notebook bonding industry.

Description

technical field [0001] The invention relates to a preparation method of an acrylate structural adhesive suitable for bonding zinc alloys, and belongs to the technical field of adhesives. Background technique [0002] Acrylic structural adhesive has many advantages such as fast curing at room temperature, good toughness and wide range of bonding materials, and is widely used in the bonding of structural parts in the electronics and electrical industries. Especially it plays an irreplaceable role in the assembly industry of notebook group structural parts. With the faster and faster upgrading of the notebook industry, various new structural parts materials are emerging in an endless stream. Among them, zinc alloy material has become a material that has attracted much attention in the notebook assembly industry due to its advantages such as low forming temperature, high processing precision, good surface quality, and fast production efficiency. However, zinc alloy materials al...

Claims

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Application Information

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IPC IPC(8): C09J4/02C09J4/06C09J11/04C09J11/06
CPCC09J4/06C09J11/04C09J11/06
Inventor 陈加立王建斌陈田安解海华
Owner YANTAI DARBOND TECH
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