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Preparation method of compact high thermal conductivity ceramic substrate

A high thermal conductivity ceramic and dense technology, which is applied in ceramic products, applications, household appliances, etc., can solve the problems of substrates prone to cracks, ceramic deformation, poor heat dissipation performance of circuit packaging boards, and low volume density of ceramic substrates, etc., to achieve thermal conductivity Enhanced, simplified preparation process and broad application prospects

Inactive Publication Date: 2018-09-04
胡果青
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem mainly solved by the present invention is that common ceramic substrates are prone to cracks, and high-temperature liquid-phase sintering will cause large deformation of ceramics during the sintering process, especially when tape-casting is used to prepare thinner substrate materials. The first defect is more obvious, which makes the volume density of the ceramic substrate small. In addition, the ceramic substrate has a defect of poor heat dissipation performance as a circuit packaging board, and a preparation method for a dense high thermal conductivity ceramic substrate is provided.

Method used

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Examples

Experimental program
Comparison scheme
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Embodiment Construction

[0024]In parts by weight, mix 30-40 parts of isophthalic acid, 20-25 parts of neopentyl glycol, 5-10 parts of trimethylolpropane, and 1-3 parts of monobutyltin oxide, and put them into a In the four-necked flask of the condensing device, start the agitator, stir at a speed of 400-450r / min, heat up to 230-250°C, and add 10-15 parts of 1,4- Cyclohexanedicarboxylic acid, acidolysis reaction for 2-3 hours, cooled to room temperature, mixed with 20-30 parts of quartz sand with a particle size of 400 mesh, continued reaction for 20-30 minutes, cooled to room temperature to obtain high thermal conductivity polyester resin; 50-60g Copper sulfate pentahydrate and 75-80g of sodium tartrate were dissolved in 200-300mL of normal temperature water respectively to obtain divalent copper solution and sodium tartrate solution, and 75g of sodium hydroxide was dissolved in 200mL of water to prepare an alkaline solution, with a volume ratio of 4ː1 , mix divalent copper solution and sodium tartra...

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Abstract

The invention discloses a preparation method of a compact high thermal conductivity ceramic substrate, and belongs to the technical field of ceramic substrates preparation. After carbon dioxide is introduced in a sodium aluminate solution, superfine aluminium hydroxide crystal grains are formed, mullite powder is doped to achieve bonding and toughening effects to avoid cracking deformation causedwhen an alumina ceramic substrate is subjected to sinter molding, and the alumina ceramic substrate is more compact. Polyester resin with high thermal deformation energy is used as a copper clad carrier, and through high stress bonding of the resin and the ceramic substrate, reliable bonding is generated; copper obtained through reduction of cuprous oxide in a hot melt coating and atoms of the ceramic substrate diffuse mutually to form a bonding layer through diffuse bonding, so that a composite plate is formed through tight bonding of the copper surface and the ceramic substrate, and an ablated metal thermal conductive layer is formed; and copper in a micro perforation of a green tape forms a thermal conductive net in the ceramic substrate, so that the thermal conductivity of the ceramicsubstrate is enhanced, and the application prospect is wide.

Description

technical field [0001] The invention discloses a preparation method of a compact high thermal conductivity ceramic substrate, belonging to the technical field of ceramic substrate preparation. Background technique [0002] Ceramic substrate refers to a special process board in which copper foil is directly bonded to the surface of an alumina or aluminum nitride ceramic substrate at high temperature. The produced ultra-thin composite substrate has excellent electrical insulation performance, high thermal conductivity, excellent solderability and high adhesion strength, and can etch various patterns like a PCB board, and has a large current-carrying capacity. ability. Therefore, ceramic substrates have become the basic materials for high-power power electronic circuit structure technology and interconnection technology. [0003] For the preparation of alumina ceramic substrates, most of the existing technologies use tape-casting technology to prepare green bodies, and then t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/185C04B35/10C04B35/622C04B41/88C04B38/02
CPCC04B35/10C04B35/185C04B35/622C04B38/02C04B41/009C04B41/5127C04B41/88C04B2235/3217C04B2235/3463C04B2235/6025C04B2235/606C04B2235/656C04B2235/6567C04B2235/658C04B2235/664C04B2235/77C04B2235/9607C04B41/455C04B41/0072
Inventor 胡果青何伟仁陈可
Owner 胡果青
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