Waterborne glass thermal insulation coating and preparation method thereof
A heat-insulating coating and glass technology, which is applied in fire-resistant coatings, reflection/signal coatings, coatings, etc., can solve problems such as poor infrared radiation rate, unstable performance, and large limitations, and achieve improved rigidity and good heat insulation effect , high stability and high temperature resistance
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Embodiment 1
[0022] The preparation method of modified potassium hexatitanate whisker:
[0023] Add potassium hexatitanate whiskers and silicon nitride into acetone, conduct ultrasonic dispersion to obtain a dispersion liquid, heat up the dispersion liquid to 75°C, then add KH560, water and polyamide in sequence, stir evenly, dry after the reaction is complete Can. The mass ratio of silicon nitride to potassium hexatitanate whiskers is 1:5, the mass ratio of KH560 to potassium hexatitanate whiskers is 1:23, and the mass ratio of polyamide to silicon nitride is 1:17 .
Embodiment 2
[0025] The preparation method of modified potassium hexatitanate whisker:
[0026] Add potassium hexatitanate whiskers and silicon nitride into acetone and perform ultrasonic dispersion to obtain a dispersion liquid. Heat the dispersion liquid to 82°C, then add KH550, water and polyamide in sequence, stir evenly, and dry after the reaction is complete. Can. The mass ratio of silicon nitride to the potassium hexatitanate whiskers is 1:5, the mass ratio of KH550 to the potassium hexatitanate whiskers is 1:20, and the mass ratio of polyamide to silicon nitride is 1 :20.
Embodiment 3
[0028] A water-based glass heat-insulating coating, calculated in parts by weight, comprises the following components:
[0029] 80 parts of a mixture of acrylic acid emulsion and silica sol, 15 parts of pure acrylic emulsion, 10 parts of nano airgel, 10 parts of modified potassium hexatitanate whiskers in Example 1, 2 parts of ammonium acrylic acid dispersant, tetrachloroisophthalate 0.8 parts of forminonitrile, 6 parts of modified ammonium polyacrylate, 2 parts of mineral oil, 9 parts of propylene glycol ether and 50 parts of deionized water.
[0030] Preparation:
[0031] 1) Add ammonium acrylate dispersant, tetrachloroisophthalonitrile, and 1 / 2 mineral oil into deionized water according to the formula amount, and stir and mix thoroughly at a speed of 300r / min;
[0032] 2) Add nano-airgel, pure acrylic emulsion and the modified potassium hexatitanate whisker of Example 1 to the mixture of step 1) and disperse at a rotating speed of 1000r / min;
[0033] 3) Add the mixture of...
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