9 results about "Indium Trichloride" patented technology

The invention discloses a preparation method of a CuInS2 / FeS2 wood mildew-proof antibacterial agent, which comprises the following steps: dissolving cuprous chloride, indium chloride tetrahydrate, ferric trichloride hexahydrate and thiourea or thioacetamide in ethylene glycol, and carrying out one-step solvothermal reaction and calcination to obtain a CuInS / FeS composite antibacterial agent; the material has triple effects of photo-thermal, photocatalysis and copper ion slow release, and can inhibit mildew and decay fungi on the surface of wood under the condition of visible-near infrared illumination or no illumination. NH4VO3 and 2-methylimidazole are added into a reaction system and calcined in an ammonia-containing atmosphere, so that a V < 5 + > / V < 4 + > redox pair can be formed on the surface, near-infrared absorption is further widened, electron-hole recombination is delayed, and long-acting antibiosis under weak light is realized. The process is simple, does not contain chromium and arsenic heavy metals, and is suitable for environmental protection of wood materials.

This invention relates to a method for preparing ZnIn2S4 adsorbents, specifically an ultrasonic atomization method based on zinc indium sulfide, belonging to the field of catalytic material preparation technology. The invention aims to address the problems of poor chemical stability and weak surface reaction kinetics in existing sulfide preparation methods. The method involves using zinc chloride, indium trichloride tetrahydrate, and thioacetamide as raw materials, and employing a hydrothermal method combined with ultrasonic atomization at 0 MHz, 1.0 MHz, 2.4 MHz, and 3.0 MHz to prepare ZIS-0, ZIS-1.0, ZIS-2.4, and ZIS-3.0 photoadsorbents, respectively. This method utilizes the acoustic cavitation, hotspot, and aggregation effects of ultrasonic atomization to achieve precise particle size control, increase specific surface area, and shorten the crystallization cycle, significantly improving the adsorption efficiency of atrazine. The preparation process of this invention is mild and simple, and the obtained materials exhibit excellent atrazine adsorption properties in aqueous solutions.

The application discloses a coated modified lithium manganese iron phosphate lithium ion battery positive electrode material, and preparation steps thereof include the following steps: (1) preparing lithium manganese iron phosphate powder; (2) mixing pyridine and hexafluorophosphoric acid, adding lithium hydroxide and ethanol, and heating in a water bath to obtain a mixture; (3) adding an aqueous solution of indium trichloride, lithium manganese iron phosphate powder and L-malic acid into an ethanol solution of cerium nitrate and n-butyl titanate at the same time, ultrasonic dispersion is carried out, then the mixed solution is laid in a container, water and ethanol are removed by drying and evaporation, calcination is carried out at 120+5 DEG C, then the mixture and selenium acid powder are added and uniformly mixed, calcination is carried out again at 650+5 DEG C, after the completion of the calcination, air cooling is carried out to normal temperature, and the coated modified lithium manganese iron phosphate lithium ion battery positive electrode material is obtained. The positive electrode material prepared by coating and modifying lithium manganese iron phosphate according to the method can significantly improve the discharge specific capacity and capacity retention rate of the battery.

The invention discloses a combined negative electrode additive for a zinc-bromine flow battery, a negative electrode electrolyte, a preparation method of the negative electrode electrolyte and the zinc-bromine flow battery, and belongs to the technical field of electrochemical energy storage, and the combined negative electrode additive for the zinc-bromine flow battery comprises indium trichloride and glycine in a molar ratio of 1: (3.33-60); during charging, indium ions in indium trichloride are reduced into metal indium on the surface of the electrode, the metal indium and the post-deposited zinc generate a nanoscale alloy layer in situ, electric field distribution is homogenized, and zinc dendritic crystal growth is inhibited; carboxyl and amino of glycine are used as electron donors to form a water-soluble complex with zinc ions, so that the reduction kinetics of the zinc ions on the surface of the electrode is slowed down; polar functional groups of glycine are adsorbed on active sites on the surface of a zinc electrode, zinc ion deposition is blocked, energy distribution of the electrode and an electrolyte interface is changed, zinc is guided to perform transverse two-dimensional growth, zinc dendrite growth is inhibited, hydroxyl ions are neutralized, and hydrogen evolution reaction is inhibited. The coulombic efficiency of the zinc-bromine flow battery is 95.4%-97.0%; the energy efficiency ranges from 81.85% to 84.49%; and the voltage efficiency is 85.8%-87.1%.

The invention discloses a nano indium adjuvant as well as a preparation method and application thereof, and belongs to the technical field of nano medicines. The preparation method comprises the following steps: mixing indium trichloride with a PVP (Polyvinyl Pyrrolidone) solution, and carrying out metal ion chelation on the mixture and a gallic acid solution to obtain the uniform and stable nano indium adjuvant. Then, the antigen ovalbumin and the nano indium adjuvant form the nano indium adjuvant vaccine, humoral immunity and cellular immunity are activated at the same time, the presentation capacity and immunogenicity of the antigen are enhanced, and the requirements of clinical anti-tumor vaccines are met.

The application relates to the technical field of nanomaterial preparation, in particular to a method for synthesizing a zinc-sulfur double-vacancy Zn3In2S6 photocatalyst, wherein specific-volume ammonia water is mixed with deionized water to form a solvent, zinc sulfate, indium trichloride and thioacetamide precursors are added, and after uniform stirring, one-step hydrothermal reaction is carried out at 160 DEG C for 12 hours, and the product is obtained through centrifugal washing and vacuum drying. Through the coordination induction effect of ammonia water, zinc vacancies and sulfur vacancies are in-situ constructed in the Zn3In2S6 crystal lattice, the introduced defect energy level is used as an electron trap to capture photo-generated electrons, carrier recombination is inhibited, and the surface active site is increased. The application can significantly improve the hydrogen production activity under visible light, the hydrogen evolution rate is 2.25 times that of the hydrogen production activity without adding ammonia water, and the application has the advantages of simple process route, excellent catalytic performance and strong structural stability.

The invention discloses preparation and application of an In2S3 nanosheet, and belongs to the field of thin film battery materials. The preparation method comprises the following steps: dissolving thioacetamide and indium trichloride in a solvent to prepare an In2S3 precursor solution, carrying out spin coating on a TiO2 nanoparticle film to form a film, and carrying out heat treatment under the protection of inert gas to obtain an In2S3 nanosheet array film; adding InCl3. 4H2O, CuI and thiourea into N, N-dimethylformamide, mixing and stirring, dropwise adding the mixture onto the In2S3 nanosheet array thin film, and spin-coating the mixture on the In2S3 nanosheet array thin film to obtain a CuInS2 precursor thin film; the CuInS2 precursor film is subjected to heat treatment, and an In2S3 / CuInS2 inorganic body type heterojunction is obtained; spin coating of a Spiro-OMeTAD solution is carried out on the In2S3 / CuInS2 inorganic body heterojunction, and after heat treatment, a Spiro-OMeTAD thin film is obtained; and a metal electrode is deposited on the Spiro-OMeTAD thin film through vapor deposition.