Waterborne glass thermal-insulation coating and preparation method thereof
A heat-insulating coating and heat-insulating filler technology, applied in coatings and other directions, can solve problems such as poor infrared radiation rate, unstable performance, and single color, and achieve stable chemical properties, good heat insulation effect, and low thermal conductivity.
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Embodiment 1
[0020] The preparation method of modified expanded perlite is:
[0021] Add expanded perlite to water containing 2wt% sodium lauryl sulfate, then add dropwise 150g / L indium trichloride solution and 60g / L zirconium oxychloride alcohol aqueous solution, stir evenly, add ammonium bicarbonate, and ultrasonically disperse Finally, precipitation is carried out, and after the precipitation is completed, water washing is carried out, and then high-temperature calcination is carried out at 600°C to 800°C to obtain modified expanded perlite. The solvent in the aqueous alcohol solution is 70% by volume of ethanol and 30% by volume of water.
Embodiment 2
[0023] The preparation method of modified expanded perlite is:
[0024] Add expanded perlite to water containing 1wt% sodium stearate, then dropwise add 100g / L indium trichloride solution and 80g / L zirconium oxychloride alcohol aqueous solution, stir evenly, add ammonium bicarbonate, perform ultrasonic dispersion treatment Precipitate, wash with water after precipitation, and then perform high-temperature calcination at 600°C to 800°C to obtain modified expanded perlite. The solvent in the aqueous alcohol solution is 50% by volume of ethanol and 50% by volume of water.
Embodiment 3
[0026] A water-based glass heat-insulating coating, calculated in parts by weight, comprises the following components:
[0027] 80 parts of the mixture of acrylic acid emulsion and silica sol, 15 parts of fluorocarbon resin, 10 parts of nano airgel, 10 parts of modified expanded perlite of embodiment 1, 2 parts of ammonium acrylate dispersant, 0.8 parts of tetrachloroisophthalonitrile 6 parts, 6 parts of modified ammonium polyacrylate, 2 parts of mineral oil, 9 parts of propylene glycol ethyl ether and 50 parts of deionized water.
[0028] Preparation:
[0029] 1) Add ammonium acrylate dispersant, tetrachloroisophthalonitrile, and 1 / 2 mineral oil into deionized water according to the formula amount, and stir and mix thoroughly at a speed of 300r / min;
[0030] 2) Add nano airgel, fluorocarbon resin and the modified expanded perlite of embodiment 1 to the mixture of step 1) and disperse at a rotating speed of 1000r / min;
[0031] 3) Add the mixture of acrylic acid emulsion and ...
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