Preparation and analysis application of electrochemical sensing device based on zinc oxide nano-rod and myoglobin
A technology of zinc oxide nanorods and myoglobin, which is applied to the electrochemical variables of materials, material analysis through electromagnetic means, scientific instruments, etc., can solve problems such as the difficulty of direct electron transfer, and achieve improved electrochemical performance and thermal stability Good performance and large specific surface area
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[0041] The preparation of Nafion / Mb-ZnONR / CILE comprises the following steps:
[0042](ⅰ) Weigh 1.6 g of graphite powder and 0.8 g of ionic liquid in a mortar and grind them thoroughly to mix them evenly, fill them into a glass electrode tube and compact them, and insert copper wires as wires to obtain CILE;
[0043] (ii) Take 8 μL of ZnONR-Mb mixture and apply it on the surface of CILE (in which the concentration of ZnONR is 0.5 mg / mL and the concentration of Mb is 15.0 mg / mL), and let it dry naturally at room temperature to obtain Mb-ZnONR / CILE;
[0044] (Ⅲ) Take 6 μL of 0.5% Nafion ethanol solution and drop-coat it on the surface of Mb-ZnONR / CILE, and let it dry at room temperature to obtain Nafion / Mb-ZnONR / CILE.
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