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Process for forming silicon carbide ceramic ball

A technology of silicon carbide ceramics and silicon carbide fine powder, which is applied in ceramic molding machines, manufacturing tools, etc., can solve problems such as being unsuitable for large-scale production, the mold cannot be used multiple times, and the number of products is small. The effect of wide and one-time investment

Inactive Publication Date: 2019-02-22
江苏高越高新科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage is that the number of products sintered in each furnace is small, and the mold cannot be used multiple times
[0008] (5) Hot isostatic pressing sintering method: Although the ceramic balls sintered by hot isostatic pressing have high density and good spherical shape, compared with other preparation methods, the cost is too high and the efficiency is low, so it is not suitable for large-scale production

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A kind of preparation method of high density silicon carbide ceramic ball, silicon carbide fine powder (a phase, median diameter 0.5um, purity is greater than 98.5%), high residual carbon phenolic resin and sintering aid (Al 2 o 3 and Y 2 o 3 Half and half) are formulated into main raw materials in proportion, and the mass percentages of each component are successively: 87% silicon carbide fine powder, 5% resin, 1.2% sintering aid, and carry out the following steps successively:

[0028] 1) Mixing: Put the main raw materials into deionized water, add binder (polyvinyl alcohol) and dispersant (tetramethylammonium hydroxide) in sequence, ball mill and mix for 12 hours, and filter through a 100-mesh screen to obtain Uniform slurry. The weight of the above-mentioned binder and dispersant is respectively 1% and 0.5% of the main raw material.

[0029] 2) Spray granulation: use a spray dryer to dry the above slurry to obtain composite granulated powder. For the spray drye...

Embodiment 2

[0033] Example 2: A method for preparing high-density silicon carbide ceramic balls. The main raw materials are made of silicon carbide fine powder, high carbon residue phenolic resin and sintering aid in proportion. The mass percentages of each component are: silicon carbide fine powder 90 %, high carbon residual phenolic resin 7%, sintering aid (B 4 C) 3%, carry out the following steps successively:

[0034] 1) Mixing: Put the main raw materials into deionized water, add binder (carboxymethyl cellulose) and dispersant (polypropylene alcohol) in sequence, ball mill and mix for 18 hours, and filter through a 140-mesh screen to obtain a uniform Slurry. The weight of the above binder and dispersant is respectively 5% and 1.5% of the main raw material.

[0035] 2) Spray granulation: use a spray dryer to dry the above slurry to obtain composite granulated powder. For the spray dryer, the hot air inlet temperature is set to 210°C, the outlet temperature is 100°C, the slurry flow...

Embodiment 3

[0039] Example 3: A method for preparing high-density silicon carbide ceramic balls. The main raw materials are made of silicon carbide fine powder, high carbon residue phenolic resin and sintering aid in proportion. The mass percentages of each component are: 95% silicon carbide fine powder Powder, 4% resin, 1% sintering aid B, follow the steps in turn:

[0040] 1) Mixing: Put the main raw materials into deionized water, add binder (dextrin) and dispersant (aluminophosphate) in turn, mix by ball milling for 24 hours, and filter through a 180-mesh screen to obtain a uniform slurry . The weight of the above-mentioned binder and dispersant is respectively 10% and 3% of the main raw material.

[0041] 2) Spray granulation: use a spray dryer to dry the above slurry to obtain composite granulated powder. For the spray dryer, the hot air inlet temperature is set to 260°C, the outlet temperature is 110°C, the slurry flow rate is 80kg / h, and the speed of the atomizer is 30Hz. The g...

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Abstract

The invention provides a silicon carbide ceramic ball. The silicon carbide ceramic ball is prepared by mixing, granulating, seeding, forming, sintering and grinding, production of seeds, forming, sintering and grinding from, by weight parts, a main ingredient and an auxiliary, wherein the main ingredient includes 87%-96% of silicon carbide fine powder, 5%-11% of high residual carbon phenolic resinand 1.2%-5% of sintering aid, wherein the sintering aid is at least one of B, C, B4C, Al2O3 and Y2O3. The auxiliary includes binder accounting for 0.9%-11% of the weight of the main ingredient and dispersing agent accounting for 0.5%-3.5% the weight of the main ingredient, and the binder is at least one of polyvinyl alcohol, dextrin and carboxymethyl cellulose; and the dispersing agent is at least one of polyethylene glycol, tetramethylammonium hydroxide, aluminophosphate, and polyacrylic acid. The silicon carbide ceramic ball has high density and stable chemical property; the silicon carbideceramic ball can meet the preparation of silicon carbide ceramic balls of multiple specifications, the range is wide, and the silicon carbide ceramic balls ranging from 1 mm to 50 mm can be produced.The one-time investment is small, and the production expansion is easy.

Description

technical field [0001] The invention relates to the field of ceramic balls and preparation methods, in particular to a molding process of silicon carbide ceramic balls Background technique [0002] Silicon carbide ceramics have high strength, low creep, friction and wear resistance, corrosion resistance and good oxidation resistance, and their excellent mechanical properties, low thermal expansion coefficient and high thermal conductivity determine the properties of silicon carbide ceramics. Thermal shock resistance is very good. Based on the above advantages, silicon carbide ceramic balls, as key components of grinding balls, ceramic bearings, and ball valves, have broad application prospects in harsh working conditions such as high temperature, strong acid, strong alkali, and impact resistance. [0003] The ball forming methods in the prior art of silicon carbide ceramic balls mainly include the following: [0004] (1) Extrusion method: The powder is sintered to obtain c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/565C04B35/622B28B1/00
CPCB28B1/00C04B35/565C04B35/622C04B2235/3217C04B2235/3225C04B2235/3821C04B2235/422C04B2235/48C04B2235/5445C04B2235/6562C04B2235/6567C04B2235/77C04B2235/94C04B2235/95
Inventor 徐辉
Owner 江苏高越高新科技有限公司
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