Process for forming silicon carbide ceramic ball
A technology of silicon carbide ceramics and silicon carbide fine powder, which is applied in ceramic molding machines, manufacturing tools, etc., can solve problems such as being unsuitable for large-scale production, the mold cannot be used multiple times, and the number of products is small. The effect of wide and one-time investment
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Embodiment 1
[0027] A kind of preparation method of high density silicon carbide ceramic ball, silicon carbide fine powder (a phase, median diameter 0.5um, purity is greater than 98.5%), high residual carbon phenolic resin and sintering aid (Al 2 o 3 and Y 2 o 3 Half and half) are formulated into main raw materials in proportion, and the mass percentages of each component are successively: 87% silicon carbide fine powder, 5% resin, 1.2% sintering aid, and carry out the following steps successively:
[0028] 1) Mixing: Put the main raw materials into deionized water, add binder (polyvinyl alcohol) and dispersant (tetramethylammonium hydroxide) in sequence, ball mill and mix for 12 hours, and filter through a 100-mesh screen to obtain Uniform slurry. The weight of the above-mentioned binder and dispersant is respectively 1% and 0.5% of the main raw material.
[0029] 2) Spray granulation: use a spray dryer to dry the above slurry to obtain composite granulated powder. For the spray drye...
Embodiment 2
[0033] Example 2: A method for preparing high-density silicon carbide ceramic balls. The main raw materials are made of silicon carbide fine powder, high carbon residue phenolic resin and sintering aid in proportion. The mass percentages of each component are: silicon carbide fine powder 90 %, high carbon residual phenolic resin 7%, sintering aid (B 4 C) 3%, carry out the following steps successively:
[0034] 1) Mixing: Put the main raw materials into deionized water, add binder (carboxymethyl cellulose) and dispersant (polypropylene alcohol) in sequence, ball mill and mix for 18 hours, and filter through a 140-mesh screen to obtain a uniform Slurry. The weight of the above binder and dispersant is respectively 5% and 1.5% of the main raw material.
[0035] 2) Spray granulation: use a spray dryer to dry the above slurry to obtain composite granulated powder. For the spray dryer, the hot air inlet temperature is set to 210°C, the outlet temperature is 100°C, the slurry flow...
Embodiment 3
[0039] Example 3: A method for preparing high-density silicon carbide ceramic balls. The main raw materials are made of silicon carbide fine powder, high carbon residue phenolic resin and sintering aid in proportion. The mass percentages of each component are: 95% silicon carbide fine powder Powder, 4% resin, 1% sintering aid B, follow the steps in turn:
[0040] 1) Mixing: Put the main raw materials into deionized water, add binder (dextrin) and dispersant (aluminophosphate) in turn, mix by ball milling for 24 hours, and filter through a 180-mesh screen to obtain a uniform slurry . The weight of the above-mentioned binder and dispersant is respectively 10% and 3% of the main raw material.
[0041] 2) Spray granulation: use a spray dryer to dry the above slurry to obtain composite granulated powder. For the spray dryer, the hot air inlet temperature is set to 260°C, the outlet temperature is 110°C, the slurry flow rate is 80kg / h, and the speed of the atomizer is 30Hz. The g...
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