Damping resin emulsion and preparation method thereof
A resin emulsion and damping technology, applied in the field of damping resin emulsion and its preparation, can solve the problems of uneven mixing of hindered phenol and acrylic resin, poor resin damping performance, narrow damping temperature range, etc., and achieves short preparation route and good damping effect. , mild reaction effect
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Embodiment 1
[0054] A kind of damping resin emulsion, calculated in parts by weight, its raw material comprises:
[0055]
[0056] Wherein, the acrylate monomer is a mixture composed of methyl acrylate, butyl acrylate and 2-ethylhexyl acrylate in a mass ratio of 2:1:0.5.
[0057] The cross-linking monomer 1 is diacetone acrylamide and adipate dihydrazide, and the mass ratio of diacetone acrylamide to adipate dihydrazide is 2:1.
[0058] The crosslinking monomer 2 is a mixture selected from diethylene glycol diacrylate, tetrahydrofuran acrylate, and ethoxylated bisphenol A dimethacrylate in a mass ratio of 1:1:0.5;
[0059] Described emulsifying agent is sodium lauryl sulfate;
[0060] The initiator is ammonium persulfate.
[0061] The raw materials of the functional acrylate monomer include: hydroxyethyl acrylate, isophorone diisocyanate, antioxidant 1010, acetone and methyl ethyl ketone mixed solvent and catalyst with a weight ratio of 50:110:170:100:0.01 , the mixed solvent of acet...
Embodiment 2
[0074] A kind of damping resin emulsion, calculated in parts by weight, its raw material comprises:
[0075]
[0076] Wherein, the acrylate monomer is a mixture composed of methyl acrylate, ethyl acrylate, butyl acrylate and 2-ethylhexyl acrylate in a mass ratio of 30:20:10:10.
[0077] The crosslinking monomer 1 is diacetone acrylamide and adipate dihydrazide, and the mass ratio of diacetone acrylamide to adipate dihydrazide is 2.5:1.
[0078] The crosslinking monomer 2 is selected from diethylene glycol diacrylate, ethoxylated bisphenol A dimethacrylate, ethoxylated trimethylolpropane triacrylate, hyperbranched polyester acrylate in a mass ratio of 1 : 1:0.5:0.3 mixture;
[0079] The emulsifier is a mixture of sodium dodecylsulfate, sodium dodecylbenzenesulfonate, and nonylphenol polyoxyethylene ether in a mass ratio of 2:2:1;
[0080] The initiator is potassium persulfate.
[0081] The raw materials of the functional acrylate monomer include: hydroxyethyl acrylate, is...
Embodiment 3
[0089] A kind of damping resin emulsion, calculated in parts by weight, its raw material comprises:
[0090]
[0091]
[0092] Wherein, the acrylate monomer is a mixture of methyl acrylate, butyl acrylate and isobornyl acrylate in a mass ratio of 2:1:1.
[0093] The crosslinking monomer 1 is diacetone acrylamide and adipate dihydrazide, and the mass ratio of diacetone acrylamide to adipate dihydrazide is 3:1.
[0094] The crosslinking monomer 2 is a mixture composed of ethoxylated bisphenol A dimethacrylate, ethoxylated trimethylolpropane triacrylate, and isobornyl acrylate in a mass ratio of 2:0.5:1;
[0095] The emulsifier is a mixture of sodium lauryl sulfate and nonylphenol polyoxyethylene ether in a mass ratio of 2:1;
[0096] The initiator is potassium persulfate.
[0097] The raw materials of the functional acrylate monomer include: hydroxyethyl acrylate, isophorone diisocyanate, antioxidant 1010, acetone and methyl ethyl ketone mixed solvent and catalyst with a w...
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