Ink and preparation method thereof
A technology of ink and magnetic nanoparticles, which is applied in the manufacture and application of ink, semiconductor/solid-state devices, etc., can solve problems such as carrier injection imbalance, affecting device luminous efficiency and stability, etc., to improve device performance and eliminate coffee Ring effect, the effect of simple method
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[0045] Another aspect of the embodiments of the present invention provides a method for preparing ink, comprising the following steps:
[0046] S01. Provide each component according to the formula of the above-mentioned ink;
[0047] S02. Disperse magnetic nanoparticles and electrode materials in an organic solvent, or disperse magnetic nanoparticles, electrode materials and surfactants in an organic solvent to obtain an ink.
[0048] The preparation method of the ink provided in the embodiment of the present invention only needs to disperse the magnetic nanoparticles and the electrode material, or the magnetic nanoparticles, the electrode material and the surfactant in the organic solvent, and the operation is simple and easy to control, and does not require strict conditions for mass production.
[0049] Specifically, in the above-mentioned step S01, the ink formula, the ratio of each component, the material and its preferred situation are as described above, and in order t...
Embodiment 1
[0061] A method for preparing ink, comprising the steps of:
[0062] S11. Provide magnetic nanoparticles Fe, electrode material Ag, mixed organic solvent and surfactant, described mixed organic solvent is made up of ethanol, 1,2-butanediol, described surfactant is ethanolamine, and various solvents all adopt The corresponding method removes water and oxygen and refines the purity to greater than 99.9%;
[0063] S12. Provide a reaction vessel such as a high-density polyethylene bottle, under the condition of stirring, add each component in the following order: 40wt% ethanol, 30wt% 1,2-butanediol, 25wt% Ag, 3wt% % Fe, 2wt% ethanolamine, and continue to stir the mixed solution for 1 h to obtain a dispersed ink.
Embodiment 2
[0065] A QLED device, comprising the following material layers sequentially stacked and combined: ITO / PEDOT:PSS (poly(3,4-ethylenedioxythiophene)-polystyrenesulfonic acid) / TFB (poly(9,9-dioctyl Base fluorene-co-N-(4-butylphenyl) diphenylamine)) / quantum dots CdSe / ZnO / magnetic electrode (Ag electrode doped with magnetic iron).
[0066] The preparation method of the QLED device is:
[0067] Prepare ITO, PEDOT:PSS layer, TFB layer, CdSe layer, ZnO layer in sequence;
[0068]The ink prepared in Example 1 was used as an electrode material, and was printed on the ZnO layer by an inkjet printing device on the ZnO layer.
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