Medical metal titanium or titanium alloy surface composite anticorrosive coating and preparation method thereof
A technology of anti-corrosion coating and surface compounding, applied in surface reaction electrolytic coating, anti-corrosion coating, coating and other directions, can solve the problems of poor adhesion between coating and substrate, uneven surface coating, difficult process control, etc. Achieve the effect of improving anti-corrosion performance, reducing elastic modulus and hardness, and strong operability
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[0024] Example 1
[0025] The preparation method of the composite anticorrosive coating on the surface of medical titanium or titanium alloy, the steps are as follows:
[0026] Step 1: Use metallic titanium or titanium alloy as the positive electrode, graphite flakes as the negative electrode, and 0.1 wt% ammonium fluoride in ethylene glycol solution as the electrolyte. Under the action of a constant voltage of 40 V, the reaction time is 1 h to complete Primary oxidation of metal. The metal titanium or titanium alloy after the primary oxidation is ultrasonically removed from the surface oxide layer, and the secondary oxidation is performed under the same conditions for a reaction time of 0.1 h to prepare a titanium dioxide nanotube layer with a regular tubular array structure. Calcination at a high temperature of 400 ℃ for 1.5h causes the titanium dioxide to change from amorphous to anatase.
[0027] Step 2: Use titanium or titanium alloy with an array layer of titanium dioxide nan...
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[0028] Example 2
[0029] The preparation method of the composite anticorrosive coating on the surface of medical titanium or titanium alloy, the steps are as follows:
[0030] Step 1: Use metallic titanium or titanium alloy as the positive electrode, graphite sheet as the negative electrode, and 2 wt% ammonium fluoride in ethylene glycol solution as the electrolyte. Under the action of a constant voltage of 80 V, the reaction time is 30 h to complete Primary oxidation of metal. The primary oxidized titanium or titanium alloy is ultrasonically removed from the surface oxide layer, and the secondary oxidation is performed under the same conditions for a reaction time of 7 hours to prepare a titanium dioxide nanotube layer with a regular tubular array structure. Calcination at a high temperature of 500 ℃ for 3.5h causes the titanium dioxide to change from amorphous to anatase.
[0031] Step 2: Use metal titanium or titanium alloy with an array layer of titanium dioxide nanotubes as t...
Example Embodiment
[0032] Example 3
[0033] The preparation method of the composite anticorrosive coating on the surface of medical titanium or titanium alloy, the steps are as follows:
[0034] Step 1: Use metal titanium or titanium alloy as the positive electrode, graphite sheet as the negative electrode, and 0.4 wt% ammonium fluoride in ethylene glycol solution as the electrolyte. Under the action of a constant voltage of 55 V, the reaction time is 5 hours to complete Primary oxidation of metal. The metal titanium or titanium alloy after primary oxidation is ultrasonically removed from the oxide layer on its surface, and the secondary oxidation is performed under the same conditions for a reaction time of 0.5 h to prepare a titanium dioxide nanotube layer with a regular tubular array structure. Calcination at a high temperature of 420 ℃ for 2h causes the titanium dioxide to change from amorphous to anatase.
[0035] Step 2: Use metal titanium or titanium alloy with an array of titanium dioxide na...
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