A long-acting washable and antibacterial fabric finishing method
A fabric finishing and washing-resistant technology, applied in the field of textile engineering, can solve the problems of fabric damage and high silver price, and achieve the effects of strong reactivity, high bonding fastness and high grafting rate.
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Embodiment 1
[0043] A method of washing fabric conditioning long-acting antimicrobial, comprising the steps of:
[0044] 1. Preparation of organic - inorganic composite lipids: the 15gN, N- di (decyl propylamino) glycine was dissolved in 100ml of triethylamine was added 15g aminopropyl triethoxysilane, condensation was added at 0 ℃ 6g hexafluorophosphate reagent benzotriazol-1-yl - yloxy tripyrrolidinophosphonium (PyBOP) reaction 6h, obtained after the completion of the reaction the organic was collected by silica gel column - inorganic complex lipid;
[0045]2, prepare an antibacterial biosilica: Weigh 0.15g organic - inorganic complex lipid, organic - inorganic complex lipid was dissolved in 10ml of chloroform, the chloroform removed by evaporation to give a lipid-based films, polycarbonate filter by liposomes extruded film extruder, the membrane pore size is 1.0 m, an antimicrobial silicon precursor solution;
[0046] 3, the cotton fabric using low temperature plasma surface treatment, cond...
Embodiment 2
[0049] A method of washing fabric conditioning long-acting antimicrobial, comprising the steps of:
[0050] 1. Preparation of organic - inorganic composite lipid: A 10g N, N- di (decyl propylamino) glycine was dissolved in 100ml of pyridine, 10g of aminopropyl triethoxysilane, 4g of condensation at -10 ℃ Reagents dicyclohexyl carbodiimide (DCC) reaction 4h, obtained after the completion of the reaction the organic collected column chromatography over silica gel - inorganic complex lipid;
[0051] 2, prepare an antibacterial biosilica: Weigh 0.1g organic - inorganic complex lipid, organic - inorganic complex lipid was dissolved in 10ml of chloroform, the chloroform removed by evaporation to give a lipid-based films, polycarbonate filter by liposomes extruded film extruder, membrane pore size of 0.5 m is, an antimicrobial silicon precursor solution;
[0052] 3, the silk fabrics using low temperature plasma surface treatment, conditions: oxygen gas is employed, the processing power o...
Embodiment 3
[0055] A method of washing fabric conditioning long-acting antimicrobial, comprising the steps of:
[0056] 1. Preparation of organic - inorganic composite lipids: the 20gN, N- di (decyl propylamino) glycine was dissolved in 100ml of triethylamine was added 20g aminopropyl triethoxysilane was added 8g condensation at 10 deg.] C Reagents N, N'- carbonyl diimidazole (CDI) reaction of 8h, obtained after the completion of the reaction the organic collected column chromatography over silica gel - inorganic complex lipid;
[0057] 2, prepare an antibacterial biosilica: Weigh 0.2g organic - inorganic complex lipid, organic - inorganic complex lipid was dissolved in 10ml of chloroform, the chloroform removed by evaporation to give a lipid-based films, polycarbonate filter by liposomes extruded film extruder, the membrane pore size is 1.0 m, an antimicrobial silicon precursor solution;
[0058] 2, the low temperature plasma linen surface treatment conditions: with nitrogen gas, the process...
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