Camellia oleosa seed oil soap base material and preparation method thereof

A technology of camellia seed oil and soap base, which is applied in the field of camellia oil soap base material and preparation thereof, can solve the problems of poor skin experience, shortened reaction time, incomplete reaction and the like of soap, and achieves short reaction time and low reaction temperature. , the effect of extending the shelf life

Pending Publication Date: 2021-01-15
江西联锴科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Another object of the present invention is to provide a preparation method of camellia oleifera seed oil soap base material, to solve the long reaction time and incomplete reaction required by the existing cold soap making technology, and the soap prepared by the traditional soap making process has poor skin experience and other problems, it can react in a lower temperature range, the reaction conditions are mild, a large amount of active ingredients in camellia oleifera oil can be retained, and a soap-based material with a pH value close to the pH value of human skin can be prepared in a short time, and because The role of the solubilizer can greatly shorten the reaction time and ensure that the active ingredients are not completely destroyed

Method used

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  • Camellia oleosa seed oil soap base material and preparation method thereof
  • Camellia oleosa seed oil soap base material and preparation method thereof
  • Camellia oleosa seed oil soap base material and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0038] (1) Boil the deionized water, after cooling, dissolve 4 parts of potassium hydroxide and 2 parts of triethanolamine in 47.99 parts of deionized water to obtain a compounded lye;

[0039] (2) Add 40 parts of Camellia oleifera seed oil and 3 parts of alkyl polyglucoside into the saponification pot, stir at a speed of 500r / min, after 10mins, add the lye compounded in step (1) into the saponification pot, After 30mins, heat up to 50°C at a rate of 5°C / min and keep it constant;

[0040] (3) After 45mins, add 0.01 part of phytic acid;

[0041] (4) After 5 minutes, stop stirring, replace the stirring and dispersing disk with an emulsifying disk, add 2 parts of sucrose fatty acid ester and 1 part of methyl p-hydroxybenzoate into the saponification pot, and emulsify for 10 minutes, stop heating and stir to room temperature;

[0042] (5) Obtain light yellow camellia oleifera seed oil soap base material, its viscosity is 7000mPa·s, and the measured pH value of 10% camellia oleif...

Embodiment 2

[0044] (1) Boil the deionized water, after cooling, dissolve 4 parts of potassium hydroxide and 2 parts of triethanolamine in 47.99 parts of deionized water to obtain a compounded lye;

[0045](2) Add 40 parts of Camellia oleifera seed oil and 3 parts of butanediol into the saponification pot, stir at a speed of 500r / min, after 10mins, add the lye compounded in step (1) into the saponification pot, after 25mins , the temperature was raised to 50°C at a rate of 5°C / min and kept constant;

[0046] (3) After 40mins, add 0.01 parts of phytic acid;

[0047] (4) After 5 minutes, stop stirring, replace the stirring and dispersing disk with an emulsifying disk, add 2 parts of sucrose fatty acid ester and 1 part of methyl p-hydroxybenzoate into the saponification pot, and emulsify for 10 minutes, stop heating and stir to room temperature;

[0048] (5) A light yellow camellia oleifera seed oil soap-based material was obtained, the viscosity of which was 7500 mPa·s, and the measured pH...

Embodiment 3

[0050] (1) Boil the deionized water, after cooling, dissolve 4 parts of potassium hydroxide and 2 parts of triethanolamine in 47.99 parts of deionized water to obtain a compounded lye;

[0051] (2) Add 40 parts of camellia seed oil and 3 parts of polyethylene glycol fatty ether into the saponification pot, stir at a speed of 500r / min, and after 10mins, add the lye compounded in step (1) into the saponification pot , after 30mins, the temperature was raised to 50°C at a rate of 5°C / min and kept constant;

[0052] (3) After 30mins, add 0.01 parts of phytic acid;

[0053] (4) After 5 minutes, stop stirring, replace the stirring and dispersing disk with an emulsifying disk, add 2 parts of sucrose fatty acid ester and 1 part of methyl p-hydroxybenzoate into the saponification pot, and emulsify for 10 minutes, stop heating and stir to room temperature;

[0054] (5) A light yellow Camellia oleifera seed oil soap-based material was obtained, the viscosity of which was 6500 mPa·s, an...

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Abstract

The invention provides a camellia oleosa seed oil soap base material and a preparation method thereof. The soap base material comprises the following components in parts by weight: 30-70 parts of camellia oleosa seed oil, 1-10 parts of a solubilizer, 1-13 parts of alkali, 1-4 parts of an emulsifier, 0.01-1 part of an antioxidant, 0.01-2 parts of a preservative and 10-50 parts of deionized water. The preparation method comprises the following steps of: (1) adding alkali into deionized water to prepare alkali liquor; (2) adding a solubilizer into the camellia oleosa seed oil, uniformly stirring,adding the alkali liquor prepared in the step (1), heating to 30-60 DEG C, and quickly stirring and saponifying for 30-90 minutes while keeping the temperature; (3) adding an antioxidant into the saponification liquid obtained in the step (2), and stirring for 5-10 minutes while keeping the temperature; and (4) adding an emulsifier and a preservative, continuing to stir for 5-15 minutes to obtaina soap base material, then stopping heating and stirring, and cooling. The camellia oleosa seed oil soap base material can react in a low temperature range within a short time, active ingredients incamellia oleosa seed oil are effectively reserved, the pH value of the soap base material is close to that of human skin, and the soap base material can be conveniently added into other systems to prepare different types of washing products.

Description

technical field [0001] The invention relates to the technical field of washing products, in particular to a camellia oleifera seed oil soap-based material and a preparation method thereof. Background technique [0002] Camellia oleifera is an evergreen oil-bearing woody plant of the family Theaceae, and people can obtain camellia oleifera seed oil by pressing, solvent leaching, and supercritical extraction of camellia oleifera seeds. Camellia oleifera seed oil is rich in oleic acid, linoleic acid, and contains a variety of unsaponifiable substances with biological activity. With the improvement of living standards, people pay more attention to their appearance and health. People are also increasingly inclined to use skin care products with natural ingredients that can improve skin condition. Vitamins, tea polyphenols, squalene and other active substances in Camellia oleifera seed oil have good antioxidant properties, but the traditional soap making process cannot effective...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11D9/02C11D9/22C11D9/26C11D9/34C11D9/38C11D9/60A61Q19/10
CPCC11D9/02C11D9/225C11D9/262C11D9/26C11D9/34C11D9/38A61Q19/10
Inventor 宁海金唐珊马江平黄尚明
Owner 江西联锴科技有限公司
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