No-clean hand sanitizer
A technology of hand sanitizer and mixed liquid, which is applied in the field of detergent composition, foam type, environmentally friendly disposable antibacterial hand sanitizer, and can solve the problems of low catalytic efficiency of cathode electrode, high energy consumption, and small amount of treated water.
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Embodiment 1
[0076] The preparation method of negative electrode comprises following preparation method:
[0077] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 5A / dm 2 , temperature 40 o C, time 30minh, inert gas atmosphere.
[0078] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 30wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1, accompanied by ultrasound Stirring 30kHz, temperature 30 o c.
[0079] (3) Place the cathode heat-treated in step (2) under the condition of inert gas for heat treatment. The heat treatment takes 12 hours and the temperature is 450 o c.
[0080] (4) Washing and drying: washing with deionized water and air drying in cold air.
[0081] Nickel salt is nickel sulfate or nickel nitrate, 15...
Embodiment 2
[0087] The preparation method of negative electrode comprises following preparation method:
[0088] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 10A / dm 2 , temperature 45 o C, time 2h, inert gas atmosphere.
[0089] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 32.5wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1.25, accompanied by Ultrasonic stirring 35kHz, temperature 33 o c.
[0090] (3) Place the cathode that has been heat-treated in step (2) under inert gas conditions for heat treatment. The heat treatment takes 18 hours and the temperature is 600 o c.
[0091] (4) Washing and drying: washing with deionized water and air drying in cold air.
Embodiment 3
[0098] The preparation method of negative electrode comprises following preparation method:
[0099] (1) Use nickel salt, aluminum salt, lanthanum salt, alkylimidazole halide, ethanedithiol as electrolyte molten salt, copper mesh or nickel mesh as cathode, high-purity aluminum plate as anode, electrodeposition condition 15A / dm 2 , temperature 50 o C, time 4h, inert gas atmosphere.
[0100] (2) Place the electrode deposited in step (2) in an alkaline solution for corrosion treatment: the alkaline solution is 35wt.% NaOH, a mixture of deionized water and ethanol with a volume ratio of 4:1.5, accompanied by ultrasound Stirring 40kHz, temperature 35 o c.
[0101] (3) Place the cathode heat-treated in step (2) under the condition of inert gas for heat treatment, the heat treatment time is 24 hours, and the temperature is 650 o c.
[0102] (4) Washing and drying: washing with deionized water and air drying in cold air.
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