Pollutant degradation and monitoring system and construction method and application thereof
A monitoring system and construction method technology, applied in the field of pollutant degradation and monitoring system, can solve the problems of expensive instruments, complicated operation, secondary pollution, etc., and achieve the effects of improved processing efficiency, simple and convenient operation, and easy portability.
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Embodiment 1
[0049] A preparation method of a gold-containing titanium dioxide nanomaterial, comprising the following steps:
[0050] Firstly, the conductive carbon cloth (CC) was pretreated, and the conductive carbon was placed in an ethanol solution containing 0.05mol tetrabutyl titanate, ultrasonicated for 20 minutes, then placed in a muffle furnace, and annealed at 400°C for 30 minutes to obtain a pre-treated carbon cloth. Treated conductive carbon cloth;
[0051] Then mix 15ml of acetone, 15ml of HCl and 1.5ml of tetrabutyl titanate, add pretreated conductive carbon cloth, transfer to the reaction kettle and put it in an oven, react at 200°C for 90 minutes, filter to obtain a precipitate, and The obtained precipitate was cleaned with distilled water and ethanol, then put into a Tris-HCl buffer solution (pH 8.5) containing dopamine (30 μg / mL), stirred for 3 hours, and filtered to obtain a precipitate, which was dried and placed in In the crucible, put it into a tube furnace, and treat...
Embodiment 2
[0053] A pollutant degradation and monitoring system includes a working electrode, a platinum electrode and a silver-silver chloride electrode. The working electrode, the platinum electrode and the silver-silver chloride electrode are respectively connected to an electrochemical workstation, and the light source is a xenon lamp.
[0054] The construction of a pollutant degradation and monitoring system comprises the following steps:
[0055] (1) Prepare the working electrode, cut the gold-containing titanium dioxide nanomaterial obtained in Example 1 into 1 cm × 1.25 cm, and use conductive glue, insulating glue and copper wire to prepare an electrode with an exposed area of 1 square centimeter. Working electrode;
[0056] (2) Connect the working electrode, the platinum electrode and the silver-silver chloride electrode to the electrochemical workstation respectively.
Embodiment 3
[0058] A pollutant degradation and monitoring system includes a working electrode, a platinum electrode and a silver-silver chloride electrode. The working electrode, the platinum electrode and the silver-silver chloride electrode are respectively connected to an electrochemical workstation, and the light source is a xenon lamp. Wherein the working electrode comprises silver-doped titanium dioxide nanoparticles prepared by T.N.Ravishankar et al. ,3493).
[0059] The construction of a pollutant degradation and monitoring system comprises the following steps:
[0060] (1) Prepare the working electrode, cut the silver-doped titanium dioxide nanoparticle material prepared by T.N.Ravishankar et al. into 1 cm × 1.25 cm, and combine it with conductive glue, insulating glue and copper wire to prepare an exposed area of 1 square centimeter. The electrode is the working electrode;
[0061] (2) Connect the working electrode, the platinum electrode and the silver-silver chloride elect...
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