EGFR gene mutation detection system and kit of detection system
A technology of EGFRT790M and system, applied in the direction of microbial measurement/inspection, DNA/RNA fragments, recombinant DNA technology, etc., can solve problems such as unsatisfactory
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Embodiment 1
[0062] Example 1 Design and establishment of EGFR gene mutation detection system
[0063] 1. Design of primer-probe combination
[0064] First, refer to the GeneBank sequence number of the EGFR (epidermal growth factor receptor) gene reported in the literature, find the gene sequence corresponding to each site from the NCBI database, and design specificity upstream and downstream of the T790M, 19DEL, and L858R mutation sites confirmed by research. Amplify the primer pair, and simultaneously design wild-type and mutant-specific probes in the case of covering the mutation site nucleotides.
[0065] Primer design principles: The primer pairs used to detect EGFR gene mutation sites T790M, 19DEL, and L858R in the present invention are designed by Primer5 and NCBI Blast software; the length of the primers is between 18-26 nucleotides, and the GC content of the primers is Between 40% and 60%, the Tm value of the primer is ≥60°C. The Tm values of each primer are roughly close to e...
Embodiment 2
[0087] Example 2 Detection of Patient Tissue Samples
[0088] Two cases of non-small cell lung cancer FFPE samples were selected, and the detection system of the present invention was used to detect the cell line DNA. The specific operation steps were as follows:
[0089] 1. DNA extraction from non-small cell lung cancer FFPE samples
[0090] Use the QIAamp DNA FFPE Tissue Kit from QIAGEN to extract DNA from non-small cell lung cancer FFPE samples, use Qubit to detect DNA concentration and quality, and finally dilute to a concentration of 10ng / μL for later use.
[0091] 2. PCR amplification
[0092] 2.1 dPCR amplification system preparation
[0093] Prepare the amplification reaction according to the system of the QIAcuity system digital PCR reaction system: 10 μL of 4×dPCR-enzyme reaction solution, 4.0 μL of 10× primer-probe mixture, 2.0 μL of FFPE DNA, and make up to 40 μL with deionized water.
[0094] 2.2 Add the reaction mixture to the sample well of the dPCR nano-micr...
Embodiment 3
[0105] Example 3 Detection of plasma free nucleic acid samples
[0106] The plasma samples of 3 patients with lung cancer were selected, and the detection system of the present invention was used to detect the plasma free nucleic acid (cfDNA). The specific operation steps are as follows:
[0107] 1. Plasma cell-free nucleic acid (cfDNA) extraction
[0108] The MagMAX™ Cell-Free DNA Isolation Kit from Applied Biosystems was used to extract cfDNA from the plasma samples of 3 lung cancer patients, and then the concentration and quality of cfDNA were detected using Qubit.
[0109] 2. PCR amplification
[0110] 2.1 dPCR amplification system preparation
[0111] Prepare the amplification reaction according to the system of the QIAcuity system digital PCR reaction system: 10 μL of 4×dPCR-enzyme reaction solution, 4.0 μL of 10× primer-probe mixture, 20.0 μL of cfDNA, and make up to 40 μL with deionized water.
[0112] 2.2 Add the reaction mixture to the sample well of the dPCR nano...
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