High-performance outdoor matte powder coating and preparation method thereof
A powder coating, high-performance technology, applied in powder coatings, anti-corrosion coatings, coatings, etc., can solve the problems of inability to achieve matting effect, poor dispersion of inorganic particles, affecting the application of powder coatings, etc., achieve good matting effect and improve weather resistance , low cost effect
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Embodiment 1
[0024] S1: Add 15 parts of sodium silicate solution into the reaction kettle, raise the temperature to 80°C, add 98% hydrochloric acid solution dropwise while stirring, adjust the pH value of the reaction system between 8.3, and the dropping rate is 1 drop / seconds, after the dropwise addition, continue the insulation reaction for 1h;
[0025] S2: Add 10 parts of talcum powder to step S1, and continue to insulate and stir the reaction for 30 minutes at a rate of 800r / min; filter and wash to obtain mixture A; add 30 parts of epoxy resin to the reaction kettle, heat up to 120°C, and stir Add 9 parts of mixture A, continue the reaction for 1 hour, and obtain the matting agent after washing, filtering, drying and crushing;
[0026] S3: Add 3 parts of cyclohexane-1,2-dicarboxylic acid diglycidyl ester to 10 parts of the matting agent described in step S2, and continue to react at a temperature of 80°C for 30 minutes; then add 30 parts of epoxy resin, 3 parts of Butyl acrylate, 5 p...
Embodiment 2
[0029] S1: Add 30 parts of sodium silicate solution into the reaction kettle, raise the temperature to 90°C, add 98% hydrochloric acid solution dropwise while stirring, adjust the pH value of the reaction system between 8.7, and the dropping rate is 3 drops / seconds, after the dropwise addition, continue the insulation reaction for 2h;
[0030] S2: Add 20 parts of talcum powder to step S1, and continue to insulate and stir the reaction for 50 minutes at a rate of 1000r / min; filter and wash to obtain mixture A; add 40 parts of epoxy resin to the reaction kettle, heat up to 140°C, and stir Add 15 parts of mixture A, continue to react for 2 hours, and obtain a matting agent after washing, filtering, drying and crushing;
[0031] S3: Add 5 parts of cyclohexane-1,2-dicarboxylic acid diglycidyl ester to 15 parts of the matting agent described in step S2, and continue to react at a temperature of 90°C for 50 minutes; then add 50 parts of epoxy resin, 8 parts of Butyl acrylate, 10 pa...
Embodiment 3
[0034] S1: Add 25 parts of sodium silicate solution into the reaction kettle, raise the temperature to 85°C, add 98% hydrochloric acid solution dropwise while stirring, adjust the pH value of the reaction system between 8.5, and the dropping rate is 2 drops / seconds, after the dropwise addition, continue the insulation reaction for 1.5h;
[0035] S2: Add 15 parts of talcum powder to step S1, and continue to insulate and stir the reaction for 45 minutes at a rate of 900r / min; filter and wash to obtain mixture A; add 35 parts of epoxy resin to the reaction kettle, heat up to 130°C, and stir Add 12 parts of mixture A, continue the reaction for 1.5h, and obtain the matting agent after washing, filtering, drying and crushing;
[0036]S3: Add 4 parts of cyclohexane-1,2-dicarboxylic acid diglycidyl ester to 12 parts of the matting agent described in step S2, and continue the reaction at a temperature of 85°C for 40 minutes; then add 40 parts of epoxy resin, 6 parts Butyl acrylate, 7...
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