Polyurethane sound insulation coating and production process thereof
A technology of sound insulation coating and production process, applied in polyurea/polyurethane coatings, anti-corrosion coatings, fire-retardant coatings, etc., can solve the problems of insufficient polyurethane strength, high production cost, unstable damping performance, etc.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0036] This embodiment provides a modified hollow glass microsphere, which is made by the following steps:
[0037] Step A1. Soak 15 g of hollow glass microspheres in 200 mL of sodium hydroxide solution with a mass fraction of 5%, stir and soak for 6 hours at a rotating speed of 200 r / min, then stop stirring and soak for 24 hours, then wash with distilled water for 3 times, filter with suction, and The cake was washed until the washing solution was neutral, and then dried in an oven at 80°C to constant weight to obtain pretreated glass beads;
[0038] Step A2. Add 0.05mol 9,9'-bis(4-hydroxyphenyl)fluorene to 190mL 1,4-dioxane, under nitrogen protection, stir and heat up to 60°C, dropwise add 0.025mol divinyldi Chlorosilane, control the dropping rate at 1 drop / second, after the dropwise addition, stir and react for 4 hours, after the reaction, remove 1,4-dioxane by rotary evaporation to obtain the intermediate product 1;
[0039] Step A3: Add 0.05 mol of pentafluoropentanethio...
Embodiment 2
[0043] This embodiment provides a modified hollow glass microsphere, which is made by the following steps:
[0044] Step A1. Soak 17g of hollow glass microspheres in 220mL of sodium hydroxide solution with a mass fraction of 8%, stir and soak for 6h at a rotating speed of 250r / min, then stop stirring and soak for 24h, then wash with distilled water for 4 times, suction filter, filter The cake was washed until the washing solution was neutral, and then dried in an oven at 80°C to constant weight to obtain pretreated glass beads;
[0045] Step A2. Add 0.05mol 9,9'-bis(4-hydroxyphenyl)fluorene to 220mL 1,4-dioxane, under the protection of nitrogen, stir and heat up to 60°C, dropwise add 0.025mol divinyldi Chlorosilane, control the dropping rate to 1 drop / second, after the dropwise addition, stir and react for 5h, after the reaction, remove 1,4-dioxane by rotary evaporation to obtain the intermediate product 1;
[0046] Step A3: Add 0.05 mol of pentafluoropentanethiol and 70 mL o...
Embodiment 3
[0050] This embodiment provides a modified hollow glass microsphere, which is made by the following steps:
[0051] Step A1, soak 18g of hollow glass microspheres in 250mL of sodium hydroxide solution with a mass fraction of 10%, stir and soak for 6h at a rotating speed of 300r / min, then stop stirring and soak for 24h, then wash with distilled water 5 times, suction filter, filter The cake was washed until the washing solution was neutral, and then dried in an oven at 80°C to constant weight to obtain pretreated glass beads;
[0052] Step A2. Add 0.05mol 9,9'-bis(4-hydroxyphenyl)fluorene to 250mL 1,4-dioxane, under nitrogen protection, stir and heat up to 60°C, dropwise add 0.025mol divinyl di Chlorosilane, control the dropping rate to 2 drops / second, after the dropping, stir the reaction for 6h, after the reaction, remove the 1,4-dioxane by rotary evaporation to obtain the intermediate product 1;
[0053] Step A3: Add 0.05 mol of pentafluoropentanethiol and 80 mL of carbon t...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com