Self-seepage concrete crack repairing glue and method for making same
A technology for repairing cracks and concrete, which is applied in building maintenance, sea area engineering, adhesive additives, etc. It can solve the problems of slow water volatilization, slow curing of repair glue, hot stickiness, cold brittleness, etc., and achieves simple preparation method and long curing time , the effect of fast curing time
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Embodiment 1
[0028] Before preparing main component A, first prepare vinyl polyurethane, concrete preparation method is as follows:
[0029] Weigh 58 grams of N-210 polyoxypropylene diol and 50 grams of diphenylmethane diisocyanate after vacuum dehydration, add them into a three-necked flask, control the temperature at 60°C and react under mechanical stirring for 2 hours, then add methacrylic acid hydroxyl 34 grams of propyl ester, heated up to 90°C and reacted for 2 hours, cooled to 25°C, and discharged to obtain vinyl polyurethane.
[0030] In a 2000ml three-necked flask, successively add 100 grams of vinyl polyurethane, 500 grams of hydroxypropyl methacrylate, 500 grams of unsaturated epoxy resin, 2.2 grams of dimethylbenzylamine and 0.5 grams of hydroquinone, and stir evenly, that is Winner component A.
[0031] Mix 49 grams of dimethyl phthalate, 36 grams of benzoyl peroxide and 2 grams of silane coupling agent, and stir evenly to obtain subcomponent B.
[0032] Test methods for pro...
Embodiment 2
[0040]In a 2000ml three-necked flask, sequentially add 300 grams of vinyl polyurethane, 600 grams of butyl methacrylate, 100 grams of unsaturated epoxy resin, 2.2 grams of dimethylbenzylamine and 0.5 grams of hydroquinone, and stir evenly, that is, the winner Component A.
[0041] Mix 49 grams of dibutyl phthalate, 36 grams of benzoyl peroxide and 30 grams of silane coupling agent, and stir evenly to obtain subcomponent B.
[0042] The test method of product performance is the same as embodiment 1.
[0043] When using, prepare the slurry according to the mass ratio of main component A: sub-component B = 50:10, mix well and inject into the crack. The glue starts to solidify in 3 minutes, and the glue solidifies completely after 10 minutes, and the crack repair is completed. The measured properties of the proportioned product in this example are: curing time of 10 minutes, viscosity of 30 cps during application, Shore D hardness of 65 at 22° C., and compressive strength of 28 M...
Embodiment 3
[0045] In a 2000ml three-necked flask, add 100 grams of vinyl polyurethane, 200 grams of methyl methacrylate, 100 grams of butyl acrylate, 600 grams of unsaturated epoxy resin, 10 grams of dimethylbenzylamine and 1 gram of hydroquinone in sequence. , Stir evenly to get the main component A.
[0046] Mix 90 grams of dimethyl phthalate, 5 grams of azobisisobutyronitrile and 5 grams of KH550 silane coupling agent, and stir evenly to obtain subcomponent B.
[0047] Test method is the same as embodiment 1.
[0048] When using, configure the slurry according to the mass ratio of main component A: sub-component B = 50:5, mix well and pour it into the crack. The glue starts to solidify in 4 minutes, and the glue solidifies completely after 15 minutes, and the crack repair is completed. The measured properties of the proportioned product in this example are: curing time 15 minutes, viscosity 50 cps when applied, Shore D hardness 55 at 22°C, and compressive strength 38 MPa.
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