Light high heat conducting nano composite material and preparation thereof
A nano-composite material and nano-material technology, applied in the field of light-weight and high-thermal-conductivity nano-composite materials and their preparation, can solve problems such as inability to meet the needs of high heat density occasions, low thermal conductivity, and difficult processing, and achieve low production costs and prices , Simple preparation process, good heat dissipation effect
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Embodiment 1
[0024] Take natural flake graphite powder, nano-silicon carbide and nano-silicon powder in a weight ratio of 70:15:15 and place them in a closed container, and mix them under stirring conditions, and the speed of the agitator is 10,000 rpm. While mixing, add polymer binder methyl cellulose with 5% of the total weight of the mixed material, and the concentration of the methyl cellulose aqueous solution is 10%. After stirring and mixing for 1 hour, the mixed material is dried at a temperature of 120°C. Disperse, and then press and sinter the powder under a vacuum of 300 degrees and a pressure of 30 MPa to obtain a light-weight and high-thermal-conductivity nanocomposite material.
[0025] It was measured that the thermal conductivity of the composite material along the hot-pressing direction was 6.1 W / m·K, and the thermal conductivity perpendicular to the hot-pressing direction was 190 W / m·K.
Embodiment 2
[0027] Pyrolytic graphite powder and nano-silicon carbide powder were placed in a closed container at a weight ratio of 85:15, and mixed under stirring conditions, and the speed of the stirrer was 11000 rpm. While mixing, add polymer binder methylcellulose with a total weight of 5% of the mixed material, and the concentration of the methylcellulose aqueous solution is 5%. After stirring and mixing for 1 hour, the mixed material is dried at a temperature of 100 ° C. Disperse, and then heat-extrude the powder in an argon atmosphere at 300 degrees and a pressure of 30 MPa to obtain a light-weight and high-thermal-conductivity nanocomposite material.
[0028] It was measured that the composite material had a thermal conductivity of 6.0 W / m·K along the extrusion direction and a thermal conductivity of 188 W / m·K along the extrusion direction.
Embodiment 3
[0030] The expanded graphite powder and nano-silicon powder are placed in a closed container in a weight ratio of 90:10, and mixed under stirring conditions, and the speed of the stirrer is 10,000 rpm. While mixing, add polymer binder polyacrylamide with a total weight of 2% of the mixed material, and the concentration of the polyacrylamide aqueous solution is 5%. After mixing and stirring for 2 hours, dry the mixed material at a temperature of 130°C, and disperse it. Then, the powder is sintered and molded under ultra-high pressure under a vacuum of 600 degrees and a pressure of 50 MPa to obtain a light-weight and high-thermal-conductivity nanocomposite material.
[0031] After measurement, the thermal conductivity of the composite material along the direction of hot pressing is 6.5W / m·K, and the thermal conductivity perpendicular to the direction of hot pressing is 228W / m·K.
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