Rare-earth halophosphate phosphor and prepration method and application thereof
A halophosphate and phosphor technology, which is applied in the field of rare earth halophosphate phosphor and its preparation, can solve the problems of powder coating process, increased difficulty of baking tube process, easy reaction with glass, shortened effective life of lamps, etc., to achieve It is beneficial to growth and development, prevention and treatment of osteoporosis, and the effect of lowering human cholesterol
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[0041] Examples 1-20: Phosphors and their preparation
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[0042] Example 1
[0043] Types and ratios of raw materials used:
[0044] La 2 O 3 : 0.830mol
[0045] MgO: 1.00mol
[0046] Gd 2 O 3 : 0.10mol
[0047] CeO 2 : 0.05mol
[0048] Nb 2 O 3 : 0.02mol
[0049] NH 4 Cl: 1.0mol
[0050] NH 4 F: 1.0mol
[0051] (NH 4 ) 2 HPO 4 : 1.0mol
[0052] Preparation method: accurately weigh the above-mentioned raw materials, and then weigh 1.0 g of H 3 BO 3 As a flux, mix it evenly, put it into a crucible, and place it in a high-temperature furnace with an oxidizing atmosphere for sintering. The above-mentioned raw materials crushed to the required particle size are put into a crucible, and placed in a high-temperature furnace with a weak reducing atmosphere for sintering, the sintering temperature is 1000-1350 ° C, and the sintering time is 1-10 hours; The phosphor powder of the present invention is obtained by washing with water, wet sieving and drying at 100-120°C. The phosphor emits UV-B ultraviolet light under the ...
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[0056] The phosphor obtained in Example 2 and the single activator phosphor (Ca, Zn) 3-x (PO 4 ) 2.14 :Gd x (B) Comparison of emission spectral power distribution, and emission spectral power distribution comparison after aging under 185nm ultraviolet light for 1000 hours, respectively image 3 and Figure 4 As shown, the former has outstanding characteristics such as high luminous efficiency, low light decay, and good chemical stability.
[0057] The rare earth halophosphate of the present invention is applied to prevent and treat osteoporosis, reduce human cholesterol and cause vitamin D deficiency 3 , various diseases caused by high cholesterol, as well as medical equipment for the treatment of psoriasis and lighting and other fields, it can be made into fluorescent physiotherapy lamps and physiotherapy devices, etc., see the following examples for details.
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