Silver-loaded copper ferrite magnetic nanometer composite fiber and preparation method and application thereof
A technology of magnetic nano and composite fibers, which is applied in botany equipment and methods, fiber treatment, fiber chemical characteristics, etc. It can solve the problems of large specific surface, difficulty in achieving antibacterial effect, high density, etc., and achieve short cycle time and low raw material price. Inexpensive and wide range of raw materials
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Embodiment 1
[0025] Embodiment 1 (silver-loaded copper ferrite fiber):
[0026] Step 1: get 3.588g copper nitrate (Cu(NO 3 ) 2 ·3H 2 O), 12.000g iron nitrate (Fe(NO 3 ) 3 .9H 2 O), 14.512g citric acid (CA:C 6 h 8 o 7 ·H 2 O), mixed in 400ml deionized water, Cu 2+ The molar concentration of Fe is 0.0371mol / L, Fe 3+ The molar concentration is 0.0743mol / L, and the raw material molar ratio is: CA: Fe 3+ :Cu 2+ =4.5:2:1, and then magnetically stirred for 24 hours.
[0027] Step 2: Then put the precursor solution into a vacuum rotary evaporator, decompress at 70°C, the pressure is about 0.05Mpa, and dehydrate for about 45 minutes to obtain a gel colloid.
[0028] Step 3: Put the gel obtained in step 2 into an oven, dry and dehydrate at 60°C, and place it in the oven for about 1 hour, then pull the gel into gel cellulose filaments, and the cellulose filaments Dry in a crucible at 100°C.
[0029] Step 4: Heat the fiber precursor to 800°C at a heating rate of 3°C / min in an air at...
Embodiment 2
[0031] Embodiment 2 (silver-loaded copper ferrite fiber):
[0032] Step 1: get 2.392g copper nitrate (Cu(NO 3 ) 2 ·3H 2 O), 8.000g ferric nitrate (Fe(NO 3 ) 3 .9H 2 O), 8.9465g citric acid (CA:C 6 h 8 o 7 ·H 2 O), mixed in 300ml deionized water, Cu 2+ The molar concentration of Fe is 0.0330mol / L, Fe 3+ The molar concentration is 0.0660mol / L, and the raw material molar ratio is: CA: Fe 3+ :Cu 2+ =4.3:2:1, and then magnetically stirred for 24 hours.
[0033] Step 2: Then put the precursor solution into a vacuum rotary evaporator, depressurize at 70°C, the pressure is about 0.05Mpa, and dehydrate for about 45 minutes to obtain a gel colloid.
[0034] Step 3: Put the gel obtained in step 2 into an oven, dry and dehydrate at 60°C, and place it in the oven for about 1 hour, then pull the gel into gel cellulose filaments, and the cellulose filaments Dry in a crucible at 100°C.
[0035] Step 4: Heat the fiber precursor to 500°C at a heating rate of 3°C / min in an air...
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