Polymer matrix composite used for liquid-oxygen containers and preparation method and using method of polymer matrix composite

A composite material and polymer technology, applied in the field of polymer-based composite materials and its preparation, can solve problems such as poor compatibility of liquid oxygen and difficulty in forming perfluoropolymer liquid oxygen containers, and achieve the effect of reducing the difficulty of forming

Inactive Publication Date: 2012-08-22
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The purpose of the present invention is to solve the problem of poor liquid oxygen compatibility of the liquid oxygen container prepared by the existing resin-based composite material, or the difficulty in

Method used

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Experimental program
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specific Embodiment approach 1

[0013] Specific Embodiment 1: This embodiment is a polymer-based composite material for a liquid oxygen container, consisting of 5-100 parts by weight of epoxy resin, 5-100 parts of benzoxazine resin, 5-100 parts of It is prepared from cyanate ester, 20-100 parts of solvent and 10-100 parts of auxiliary agent.

specific Embodiment approach 2

[0014] Specific embodiment two: the difference between this embodiment and specific embodiment one is: the epoxy resin is glycidyl ether epoxy resin, glycidyl ester epoxy resin, novolac epoxy resin or silicone epoxy resin; The benzoxazine resin is aniline benzoxazine resin or MDA benzoxazine resin; the cyanate is bisphenol A cyanate or bisphenol F cyanate; the solvent It is acetone, toluene, ethanol or long-chain aliphatic hydrocarbon; the described auxiliary agent consists of 1-100 parts by weight of inorganic filler, 1-100 parts of toughening agent, 1-20 parts of antioxidant, 1-40 parts of inhibitor Combustion agent and 0.5 to 10 parts of accelerator are mixed. Others are the same as in the first embodiment.

specific Embodiment approach 3

[0015] Specific embodiment three: the difference between this embodiment and specific embodiment two is: the inorganic filler is selected from silicon micropowder, alumina powder, calcium oxide powder, calcium carbonate powder, asbestos powder, feldspar powder, mica powder and antimony White powder; the toughening agent is selected from nitrile rubber, polysulfide rubber, hydroxyl-terminated polybutadiene, polyurethane elastomer, polyurea, liquid crystal epoxy, polyetheretherketone, polyethersulfone, polyetherimide and polyphenylene ether; the antioxidant is metal ion chelate, phosphate; the flame retardant is aluminum hydroxide, magnesium hydroxide, halogen flame retardant; the accelerator is imidazole, 2 - Ethyl 4-methylimidazole, 1-methylimidazole or an organometallic complex. Others are the same as in the second embodiment.

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Abstract

A polymer matrix composite used for liquid-oxygen containers and a preparation method and a using method of the polymer matrix composite relate to polymer matrix composite and a preparation method thereof. Aiming to solve the problems that existing liquid-oxygen containers made of resin matrix composite are poor in liquid oxygen compatibility or liquid-oxygen containers made of perfluor polymer are difficult in forming. The polymer matrix composite used for the liquid-oxygen containers is made of epoxy resin, benzoxazine resin, prussic acid fat, solvent and auxiliaries. The preparation method includes: firstly, weighing; secondly, preparing prussic acid fat prepolymer; thirdly, fusing and mixing to obtain epoxy/benzoxazine rubber solution; and fourthly, preparing the rubber solution. The using method includes: firstly, subjecting to impregnation, forming by combining a winding forming method, a vacuum bag hot-pressing tank forming method and a hang-pasting forming method, curing by a gradient-heating curing method, and finally performing thermal treatment, and obtaining a liquid-oxygen container. The polymer matrix composite is mainly used for preparing liquid-oxygen containers.

Description

technical field [0001] The invention relates to a polymer-based composite material and a preparation method thereof. Background technique [0002] The basic technology of composite cryogenic liquid oxygen container originated from the late 1980s to the early 1990s, and was first developed by the United States for the development of high-performance spacecraft. [0003] Compared with the traditional all-metal material liquid oxygen container, the polymer matrix composite material cryogenic liquid oxygen container has many advantages such as light weight, high pressure bearing, and safe failure mode of leakage before bursting. These advantages of composite material low-temperature liquid oxygen container will make it widely used in various industrial sectors in the future: clean energy vehicles powered by hydrogen-oxygen fuel cells have become the development trend of clean energy transportation in the future; steelmaking requires a large amount of oxygen; mobile Industries s...

Claims

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Application Information

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IPC IPC(8): C08L63/00C08L79/04C08K7/00C08K7/06C08K7/14C08K3/34C08K3/22C08K3/26C08G79/06B29C70/28B29C70/44B29C70/30
Inventor 赫晓东王荣国刘文博张辰威矫维成扬帆郝立峰张剑光徐忠海
Owner HARBIN INST OF TECH
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