Preparation method for one-component waterborne polyurethane transparent heat-insulating coating
A technology for water-based polyurethane and thermal insulation coatings, applied in the direction of polyurea/polyurethane coatings, coatings, etc., can solve the problems of time-consuming and energy-consuming, complex process and technology, and achieve convenient construction, simple preparation process, and improved compatibility. Effect
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[0027] Example 1
[0028] Toluene diisocyanate (TDI) and polyoxypropylene glycol with a molecular weight of 2000 are dehydrated into a four-necked flask at a weight ratio of 1:4, protected by nitrogen, and added dibutyltin dilaurate (0.2% of the resin mass fraction), React at 80°C for 2 hours, add chain extender ethylene glycol and dimethylolbutyric acid (accounting for 4% of resin mass fraction) at 50°C, then react at 80°C for 4 hours; add methyl ethyl ketone (accounting for resin mass fraction 50 %) Reduce the viscosity of the system and cool to 30°C, add triethylamine (2.4% of the resin mass fraction) dropwise under high-speed stirring, react for 20 minutes, add dropwise silane coupling agent γ-(β-aminoethyl)aminopropyltrimethyl Oxysilane (accounting for resin mass fraction 2.5%), control it to drip within 1 hour, and react at 70°C for 2 hours; disperse nano-powder antimony tin oxide (accounting for resin mass fraction 10%) in water in advance, and ultrasound For 1 hour, add ...
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[0029] Example 2
[0030] The diphenylmethane diisocyanate (MDI) and the polycarbonate polyol with a molecular weight of 2000 are dehydrated into a four-necked flask at a weight ratio of 1:5, protected by nitrogen, and triethylenediamine (accounting for 0.3% of the resin mass fraction) ), react at 70°C for 1 hour, add chain extender ethylene glycol and dimethylolpropionic acid (which account for 5% of the resin mass fraction) at 40°C, then react at 60°C for 4 hours; add methyl ethyl ketone (account for resin Mass fraction 45%) Reduce the viscosity of the system to 30°C, add triethylamine (2.5% of the resin mass fraction) dropwise under high-speed stirring, react for 10 minutes, add dropwise silane coupling agent γ-(2,3-propylene oxide) ) Propyl trimethoxysilane (accounting for 3% of the resin mass fraction), control it to drip within 1 hour, and react at 60°C for 2 hours; disperse the nano powder indium tin oxide (accounting for 8% of the resin mass fraction) in advance In water...
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