Preparation method for plastic hollow globule, and prepared product and application thereof

A hollow ball and plastic technology, applied in the field of plastic processing, can solve problems such as deformation, low glass transition temperature of polystyrene, loss of hollow structure, etc.

Active Publication Date: 2014-02-19
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the low glass transition temperature of polystyrene, about 90-100°C, it is easy to deform and lose its hollow structure under high temperature and high pressure,

Method used

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  • Preparation method for plastic hollow globule, and prepared product and application thereof
  • Preparation method for plastic hollow globule, and prepared product and application thereof
  • Preparation method for plastic hollow globule, and prepared product and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0064] Example 1

[0065] Collect the waste plastic whose main component is polycarbonate, clean it and dry it for later use.

[0066] (1) Configure the oil phase: Weigh 3.75g of the above polycarbonate and add it to 93g of chloroform. After the polycarbonate is completely dissolved, stir evenly as the oil phase (O); the oil phase solute accounts for 4% of the weight of the organic solvent , The weight percentage of polycarbonate plastic in the oil phase solute is 100%;

[0067] (2) Configure the first aqueous phase: take 8ml of distilled water, add 0.16g of sodium dodecyl sulfonate, completely dissolve and stir evenly, as the first aqueous phase (W1); wherein the weight of the emulsifier accounts for 2% of the weight of the water;

[0068] (3) Configure the second aqueous phase: take 400ml of distilled water, add 0.48g of gelatin, 0.4g of sodium dodecylbenzene sulfonate, completely dissolve and stir evenly, as the second aqueous phase (W2); where the weight of the dispersant accounts...

Example Embodiment

[0073] Example 2

[0074] Collect the waste plastic whose main component is polycarbonate, clean it and dry it for later use.

[0075] (1) Preparation of oil phase: Weigh 6g of the above polycarbonate and add it to 93g of dichloromethane. After the polycarbonate is completely dissolved, add 0.3g of plasticizer dibutyl phthalate, and stir evenly as the oil phase (O ); Among them, the oil-phase solute accounts for 6.5% of the weight of the organic solvent, the oil-phase solute contains 100% of the weight of polycarbonate plastic, and the amount of plasticizer is 5% of the weight of the polycarbonate;

[0076] (2) Configure the first aqueous phase: take 55ml of distilled water, add 4.4g of sodium dodecylbenzene sulfonate, completely dissolve and stir evenly, as the first aqueous phase (W1); wherein the weight of emulsifier accounts for 8% of the weight of water;

[0077] (3) Configure the second aqueous phase: take 640ml of distilled water, add 12.8g of xanthan gum, 0.48g of sodium laury...

Example Embodiment

[0082] Example 3

[0083] Collect the waste plastic whose main component is polycarbonate, clean it and dry it for later use.

[0084] (1) Preparation of the oil phase: weigh 15g of the above polycarbonate and add it to 93g of benzene. After the polycarbonate is completely dissolved, add 1.5g of plasticizer dioctyl terephthalate, and stir evenly as the oil phase (O); Among them, the oil-phase solute accounts for 16% of the weight of the organic solvent, the oil-phase solute contains 100% of the weight of polycarbonate plastic, and the amount of plasticizer is 10% of the weight of the polycarbonate;

[0085] (2) Configure the first aqueous phase: take 32ml of distilled water, add 0.96g of sorbitan oleate, completely dissolve and stir evenly, as the first aqueous phase (W1); wherein the weight of the emulsifier accounts for 3% of the weight of the water;

[0086] (3) Configure the second aqueous phase: take 1350ml of distilled water, add 74g of carboxymethyl cellulose, completely dissol...

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Abstract

The invention provides a preparation method for a plastic hollow globule and the prepared plastic hollow globule and application thereof. The preparation method comprises the following steps: dissolving an oil phase solute in an organic solvent to obtain an oil phase, wherein the oil phase solute is polycarbonate or a mixture of polystyrene and/or a styrene monomer and polycarbonate; adding an emulsifier into water to obtain a first water phase; adding a dispersant or a mixture of the dispersant and the emulsifier into water to obtain a second water phase; fully emulsifying the oil phase and the first water phase to prepare a first emulsion; adding the second water phase into the first emulsion for complete emulsification so as to obtain a second emulsion and heating the second emulsion to allow the organic solvent to evaporate and an oil phase liquid drop to be cured and foamed; and carrying out liquid-solid separation, separating out a solid phase and drying the solid phase to prepare the plastic hollow globule with a hollow structure inside and an average particle size of 1 to 300 mu. The plastic hollow globule has a small and controllable particle size and can be used in fields like oil drilling fluids, cosmetics and paints.

Description

technical field [0001] The invention relates to the field of plastic processing, and more specifically, relates to a method for preparing hollow plastic pellets, products prepared by the same and applications thereof. Background technique [0002] Hollow microsphere materials have unique chemical and physical properties due to their special hollow structure. In recent years, they have attracted more and more attention and become a research hotspot in the field of materials. So far, inorganic materials, polymer materials, metal oxide materials and semiconductor materials (gallium oxide, gallium nitride) have all been tried to be prepared into hollow microsphere materials by domestic and foreign researchers. Different special features for solid materials. These hollow microsphere materials with special characteristics are expected to be used in microreactors, drug delivery, controlled release, photocatalysis, enzyme coating, photonic crystals, etc. In addition, due to the lo...

Claims

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Application Information

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IPC IPC(8): B01J13/02B01J13/14C08F112/08
Inventor 陈铖常连玉赵素丽刘贵传安生高书阳柴龙
Owner CHINA PETROLEUM & CHEM CORP
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