Hydrophilic double-component grouting plugging material
A leakage plugging material and two-component technology, applied in the field of high-performance hydrophilic polyurethane/water glass two-component grouting plugging material and its preparation, can solve the problem of insufficient curing time, poor stability of consolidated body, and adjustable The problem of small range, etc., to achieve the effect of efficient water blocking and water blocking performance, fast gel speed, and improving water blocking efficiency.
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[0037] Example 1
[0038] (1) Weigh 95g high hydrophilic polyether polyol (functionality 3, molecular weight 6000, EO / PO=75:25), 5g polyvinyl alcohol 2000, and 10g DBP together into the reaction kettle, under vacuum degree -0.08MPa , vacuum dehydration at 115 °C for 2 h; after cooling to 60 °C, add 20 g of toluene diisocyanate to the reaction kettle under nitrogen atmosphere, and react for 3 h; add 0.1 g of triethylamine to the reaction kettle and continue to react for 1 h, and cool down to 50 ° C Then, 60 g of propylene carbonate and 0.02 g of benzenesulfonyl chloride were added to the reaction kettle under a nitrogen atmosphere, and the mixture was stirred for 20 minutes and then discharged to obtain component A.
[0039] (2) Dissolve 0.5 g of stannous octoate and 5 g of diethylenetriamine in 100 g of water glass solution (the mass fraction of sodium silicate is 30%, and the modulus of sodium silicate is 3.5) to obtain component B.
[0040] (3) Mix component A and component...
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[0045] Example 2
[0046] (1) Weigh 80g high hydrophilic polyether polyol (functionality 3, molecular weight 8200, EO / PO=80:20), 20g PTMEG1000, and 50g DOP, and add them to the reaction kettle together. Under the condition of ℃, vacuum dehydration for 2 hours; after cooling to 60 ℃, add 9 g of toluene diisocyanate to the reaction kettle under nitrogen atmosphere, and react for 3 hours; keep 60 ℃, add 31 g of liquefied diphenylmethane diphenyl to the reaction kettle under nitrogen atmosphere Isocyanate, continue to react for 1h; add 0.3g dibutyltin dilaurate to the reaction kettle and continue to react for 1h, after cooling to 50 ℃, add 20g mixed dibasic acid ester and 0.05g anhydrous phosphoric acid to the reaction kettle under nitrogen atmosphere, After stirring for 10~30min, the material is discharged to obtain component A.
[0047] (2) Dissolve 2g triethylamine and 2g triethanolamine in 100g water glass solution (the mass fraction of sodium silicate is 30%, and the modulus...
Example Embodiment
[0053] Example 3
[0054] (1) Weigh 90g high hydrophilic polyether polyol (functionality 3, molecular weight 10000, EO / PO=95:5), 10g polyvinyl alcohol 200, 30g DOP and add them to the reaction kettle together, under vacuum degree -0.08 MPa, vacuum dehydration at 115°C for 2h; after cooling to 60°C, add 27.6g of toluene diisocyanate to the reaction kettle under nitrogen atmosphere, and react for 3h; keep 60°C, add more than 33.4g to the reaction kettle under nitrogen atmosphere Phenyl polymethylene polyisocyanate, continue to react for 1h; add 0.23g of 2,2-bismorpholinyl diethyl ether to the reaction kettle and continue to react for 1h, after cooling to 50 ℃, add 0.23g to the reaction kettle under nitrogen atmosphere 40g of 1,2-propanediol carbonate and 0.03g of tartaric acid were added, and the mixture was stirred for 10-30min and then discharged to obtain component A.
[0055] (2) Dissolve 1 g of N,N-dimethylbenzylamine and 4 g of m-phenylenediamine in 100 g of water glass s...
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