Silver antibacterial breathable water absorbing acrylic ester foam material and preparation method and application thereof

A technology of water-absorbing acrylate and foam materials, applied in absorbent pads, medical science, bandages, etc., can solve the problems of easy breeding of bacteria, insufficient air permeability, itchy skin, etc., achieve good water absorption, good antibacterial performance, and improve air permeability performance effect

Inactive Publication Date: 2015-07-08
佛山市联塑万嘉新卫材有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, when sanitary products are contaminated by body fluids such as urine, bacteria are likely to breed, which can easily cause

Method used

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  • Silver antibacterial breathable water absorbing acrylic ester foam material and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0051] S1. Prepare the oil phase system, weigh 7.2g of isooctyl acrylate, 0.8g of isooctyl methacrylate, 4.8g of ethylene glycol dimethacrylate, 0.4g of hexanediol diacrylate, and 1.6g of carbon dioxide Silicon-loaded silver antibacterial agent, Tween-80 1.2g, stir the oil phase evenly for use, wherein the mass ratio of isooctyl acrylate to isooctyl methacrylate is 9:1.

[0052] S2. Prepare the water phase system, weigh 0.096g of calcium chloride, add water to 480g to dissolve it, at this time, the mass fraction of the electrolyte is 0.02%, and set aside; prepare the initiator phase, weigh 1.71g of ammonium persulfate , add water to 10g to dissolve, set aside.

[0053] S3. Transfer 320 g of the prepared water phase into a 1000 ml three-necked flask, start stirring, raise the temperature to 75° C., and stir at a speed above 800 rpm, then add the uniformly stirred oil phase and 0.32 g of light calcium carbonate into the three-necked flask , before the emulsion becomes viscous, ...

Embodiment 2

[0056] S1. Prepare the oil phase system, weigh 7g of isooctyl acrylate, 1g of isooctyl methacrylate, 4.8g of ethylene glycol dimethacrylate, 0.4g of hexanediol diacrylate, and 1.6g of silica-loaded Silver antibacterial agent, Tween-80 1.2g, stir the oil phase evenly for use, wherein the mass ratio of isooctyl acrylate to isooctyl methacrylate is 7:1.

[0057] S2. Prepare the water phase system, weigh 0.096g of calcium chloride, add water to 480g to dissolve it, at this time, the mass fraction of the electrolyte is 0.02%, and set aside; prepare the initiator phase, weigh 1.71g of ammonium persulfate , add water to 10g to dissolve, set aside.

[0058] S3. Transfer 320 g of the prepared water phase into a 1000 ml three-necked flask, start stirring, raise the temperature to 75° C., and stir at a speed above 800 rpm, then add the uniformly stirred oil phase and 0.32 g of light calcium carbonate into the three-necked flask , before the emulsion becomes viscous, add 160g of the wate...

Embodiment 3

[0061] S1. Prepare the oil phase system, weigh 12g of isooctyl acrylate, 1.5g of isooctyl methacrylate, 0.4g of ethylene glycol dimethacrylate, 0.4g of hexanediol diacrylate, and 0.8g of silica Load silver antibacterial agent, Tween-80 0.8g, stir the oil phase evenly for use, wherein the mass ratio of isooctyl acrylate to isooctyl methacrylate is 8:1.

[0062] S2. Prepare the water phase system, weigh 0.096g of calcium chloride, add water to 480g to dissolve it, at this time, the mass fraction of the electrolyte is 0.02%, and set aside; prepare the initiator phase, weigh 1.71g of ammonium persulfate , add water to 10g to dissolve, set aside.

[0063] S3. Transfer 320 g of the prepared water phase into a 1000 ml three-necked flask, start stirring, raise the temperature to 75° C., and stir at a speed above 800 rpm, then add the uniformly stirred oil phase and 0.32 g of light calcium carbonate into the three-necked flask , before the emulsion becomes viscous, add 160g of the wat...

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Abstract

The invention discloses a silver antibacterial breathable water absorbing acrylic ester foam material and a preparation method and application thereof. The prepared foam foam material has small pore size, and average deionized water absorption rate, average salt water absorption rate, average artificial urine absorption rate and average artificial blood rate greater than 18 g/g, 1 h water retention higher than 85%, ans is applicable to dispersion and storage of aqueous fluid. In addition, due to the addition of silver antibacterial particles, the foam material has good antibacterial property, and has antibacterial rate on colibacillus and Staphylococcus aureus higher than 95%; due to the addition of light calcium carbonate, the material has gas transmission rate greater than 1.5*10<-2> cm<3> / (m2.Pa.d) and shows good permeability. Therefore, the massive soft water absorbing material is particularly applicable to the field of sanitary products.

Description

technical field [0001] The invention belongs to the field of water-absorbing materials, and in particular relates to a silver antibacterial breathable water-absorbing acrylate foam material and a preparation method and application thereof. Background technique [0002] In today's hygienic products, the water-absorbing material inside is mainly granular synthetic resin. After absorbing water, urine or blood, it will form a gel, which is easy to form agglomerates, making it difficult to fix in one position. It is very uncomfortable in the actual use process. Comfortable. Therefore, it is of great significance to develop block-shaped soft water-absorbing materials. [0003] Normal blood is composed of blood cells, plasma, etc. The diameter of blood cells is about 8 μm, and the diameter of acrylic acid molecules is much smaller than that of blood cells. Therefore, blood cells are not easily absorbed by the gel-like superabsorbent resin, and can only stay on the surface of the...

Claims

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Application Information

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IPC IPC(8): C08F220/18C08F222/14C08F222/20C08F2/24C08K9/12C08K3/08C08K3/26C08J9/28A61L15/24A61L15/46A61L15/42
Inventor 梁永江
Owner 佛山市联塑万嘉新卫材有限公司
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