Manufacturing method of composite tungsten oxide nanoparticle, infrared absorbing material and infrared shielding body
A manufacturing method and nanoparticle technology, applied in radiation-absorbing coatings, tungsten oxide/tungsten hydroxide, nanotechnology, etc., can solve the problems of high cost and low production efficiency
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[0035] Further, the present invention also provides an infrared shielding body, which is made by mixing a nano-slurry formed by mixing the above-mentioned infrared absorbing material and a dispersing agent with a resin. In this embodiment, the preparation method of the infrared shielding body may include the following steps: first, mixing the above-mentioned external radiation absorbing material and a dispersant in a suitable solvent, wherein the dispersant may be a polymer acid, a polymer alkali or high molecular neutral dispersant; then, wet grinding is applied to the mixture obtained in the previous step to form a nano-slurry; after that, after mixing the nano-slurry with a medium resin, it is coated on a substrate For the surface, the media resin can be used alone or in combination with a thermosetting resin, an ultraviolet curing resin, an electron beam curing resin, a normal temperature curing resin, a thermoplastic resin, and the like.
[0036] In order for those skille...
Example Embodiment
[0037] Experimental Example 1: Directly dissolve tungsten hexachloride, cesium hydroxide and potassium hydroxide in an aqueous ethanol solution, and add an appropriate amount of water in a dropwise manner until precipitation occurs. Its chemical reaction formula is as follows:
[0038] WCl 6 +H 2 O+CsOH+KOH→WOCl 4 +K + +Cs + +HCl+H 2 O
[0039] WOCl 4 +Cs + +K + +HCl→WO 3 (↓)+Cs + +K + +6HCl
[0040] Then use supergravity to separate most of the solution from the precipitate to obtain a muddy precipitate (gel), and then extract the solvent into a dry powder in a vacuum oven. The dry powder of cesium tungsten oxychloride is placed in a high temperature furnace, and the A certain proportion of passivation gas and hydrogen can reduce the composite tungsten potassium cesium oxychloride to tungsten potassium cesium oxide. The process conditions are as follows: in a high temperature furnace at a heating rate of 3 to 5°C per minute, the temperature is raised from room tem...
Example Embodiment
[0043] Example 2: Directly dissolving tungsten hexachloride, cesium hydroxide and rubidium hydroxide in an aqueous ethanol solution, and adding an appropriate amount of water in a dropwise manner until precipitation occurs. Its chemical reaction formula is as follows:
[0044] WCl 6 +H 2 O+CsOH+RbOH→WOCl 4 +Rb + +Cs + +HCl
[0045] WOCl 4 +Cs + +Rb + +HCl→WO 3 (↓)+Cs + +Rb + +6HCl
[0046] Then, use supergravity to separate most of the solution from the precipitate to obtain a muddy precipitate, and then extract the solvent into a dry powder with a vacuum oven. gas and hydrogen to reduce the composite tungsten potassium oxychloride to cesium tungsten oxide. The process conditions are as follows: in a high temperature furnace at a heating rate of 3 to 5°C per minute, the temperature is raised from room temperature to 580°C, and sintered at a constant temperature of 580°C for 2 hours. Thus can obtain the composite tungsten oxide crystal that contains cesium, potass...
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