Polyurethane-based cellular material compounding vessel growth promotion factors and preparation method of polyurethane-based cellular material
A technology of vascular growth factor and polyurethane, which is applied in medical science, absorbent pads, bandages, etc., can solve the problems of loss of biological activity and short half-life, and achieve the effect of promoting skin tissue repair, promoting wound angiogenesis, and good repeatability
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Embodiment 1
[0037] (1) Preparation of polyurethane prepolymer: Add 150g ethylene oxide / propylene oxide random polymer (average molecular weight 2kD, ethylene oxide content 80%) and 18g toluene diisocyanate into a round bottom flask, Mechanically stir and mix evenly, heat to 60° C., and react for 6 hours to generate a polyurethane prepolymer with isocyanate end groups. In an intermediate stage of the reaction, the product is sampled and the content of isocyanate groups is determined according to the titration method using n-butylamine standard solution.
[0038] (2) Preparation of polyurethane porous material of complex glycosaminoglycan: mix 50wt% of polyurethane prepolymer obtained in step (1), 39wt% of distilled water as foaming agent, 10wt% of sorbitol as crosslinking agent and 1wt% heparin (use after making 10mg / mL solution). The resulting mixture was stirred at a speed of 3000 rpm for 30 seconds, transferred to a pre-shaped mold, and foamed at 40°C for 15 minutes to obtain a polyure...
Embodiment 2
[0041]Step (1) Preparation of polyurethane prepolymer: The isocyanate used is diphenylmethane diisocyanate, xylene diisocyanate or hexamethylene diisocyanate, and the others are the same as in Example 1.
Embodiment 3
[0043] Step (1) Preparation of polyurethane prepolymer: a random polymer of ethylene oxide and propylene oxide (the average molecular weight is 2kD, and the content of ethylene oxide is 50%). Others are the same as in Example 1.
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