A three-dimensional fiber reinforced lightweight non-combustible thermal insulation composite material and its preparation method
A thermal insulation and fiber-reinforced technology, which is applied in the field of lightweight non-combustible thermal insulation composite materials and its preparation, can solve the problems of construction difficulties, rock wool dust endangering workers' health, poor thermal insulation performance, etc., and achieves a high degree of mechanization and automation. Excellent high temperature shape retention ability and the effect of improving fire resistance
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[0024] When preparing the three-dimensional fiber-reinforced lightweight non-combustible thermal insulation composite material of the present invention, first select the three-dimensional fiber reinforcement, impregnate the resin solution, control the amount of solution impregnated to form a composite, then heat and dry for a certain period of time, and then apply pressure and solidify The blank is made for a certain period of time, and finally the product of the target size is obtained by machining the shape of the blank. The preparation process is as figure 1 As shown, a method for preparing a three-dimensional fiber-reinforced lightweight non-combustible thermal insulation composite material comprises the following steps:
[0025] (1) Select three-dimensional silicon-based fiber, three-dimensional basalt fiber or a three-dimensional fiber reinforcement mixed in any proportion according to the target performance and size of the product; the thickness of the three-dimensional...
Embodiment 1
[0032] The steps of the preparation method of the golden insulation board with a size of 300×300×10 are as follows:
[0033] (1) Choose a three-dimensional knitted basalt fiber reinforcement with a size of 330×330×15 and a density of 0.14g / cm3;
[0034] (2) choose phenolic novolac resin as solute, choose ethanol as solvent, choose oxalic acid as curing agent, stir by paddle and make resin dissolve completely, prepare the solution that contains 8wt% phenolic phenolic resin, and add curing agent and stir, the content of curing agent Weight is 4wt% of aminophenol-formaldehyde resin;
[0035](3) fully immersing the three-dimensional fiber reinforcement selected in step (1) into the solution prepared in step (2);
[0036] (4) Squeeze out excess solution in the composite body formed by dipping in step (3), and control the weight percentage of the three-dimensional fiber reinforcement in the composite body after extrusion of excess solution to be 45wt%;
[0037] (5) Dry the composi...
Embodiment 2
[0042] The implementation steps of the preparation method of the tan insulation board whose size is 600×600×25 are as follows:
[0043] (1) Choose a three-dimensional woven silicon-based fiber reinforcement with a size of 630×630×30 and a density of 0.09g / cm3;
[0044] (2) choose barium phenolic resin as solute, choose propanol as solvent, choose benzenesulfonic acid as solidifying agent, stir by paddle to make resin dissolve completely, prepare the solution that contains 5wt% barium phenolic resin, and add solidifying agent and stir , the weight of curing agent is 2.5wt% of barium phenolic resin;
[0045] (3) fully immersing the three-dimensional fiber reinforcement selected in step (1) into the solution prepared in step (2);
[0046] (4) Squeeze out excess solution in the composite body formed by dipping in step (3), and control the weight percentage of the three-dimensional fiber reinforcement in the composite body after extruding the excess solution to be 40wt%;
[0047]...
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