A perovskite solar cell based on metal nanoparticle interface modification and its preparation method
A technology of metal nanoparticles and solar cells, applied in the field of solar cells, can solve problems such as insufficient absorption, and achieve the effects of improving photoelectric conversion efficiency, high short-circuit current, and high photoelectric conversion efficiency
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Embodiment 1
[0026] according to figure 1 Schematic diagram of the structure of the perovskite solar cell device for device preparation.
[0027] The commercial ITO was sonicated in an ultrasonic cleaning machine for 15 minutes each through acetone, detergent, deionized water and isopropanol, then dried with a nitrogen stream, and then treated with ozone for 20 minutes.
[0028] Place the cleaned and ozone-treated ITO glass on a spin coater, spin-coating at a speed of 3000 revolutions per minute to prepare the hole transport layer PEDOT:PSS, and then anneal it on a 150 degree heating stage for 15 minutes.
[0029] Au@SiO 2 Nanoparticles were prepared into ethanol solutions with concentrations of 0.032pM, 0.047pM and 0.095pM, and then sonicated for 5 minutes, fully dispersed, spin-coated on the PEDOT:PSS layer at a speed of 3000 rpm, and then annealed at 120 degrees for 5 minutes , Au@SiO prepared 2 The morphology and size distribution of the nanoparticle layer are as figure 2 , image 3 with Fi...
Embodiment 2
[0038] The commercial ITO was sonicated in an ultrasonic cleaning machine for 15 minutes each through acetone, detergent, deionized water and isopropanol, then dried with a nitrogen stream, and then treated with ozone for 20 minutes.
[0039] Place the cleaned and ozone-treated ITO glass on a spin coater, spin-coating at a speed of 3000 revolutions per minute to prepare the hole transport layer PEDOT:PSS, and then anneal it on a 150 degree heating stage for 15 minutes.
[0040] Au@SiO 2 The nanoparticles were prepared into an ethanol solution with a concentration of 0.047pM, then sonicated for 5 minutes, fully dispersed, and then spin-coated on the PEDOT:PSS layer at a speed of 3000 rpm, and annealed at 120 degrees for 5 minutes.
[0041] Mix lead bromide and bromomethylamine into a DMF solution with a concentration of 500mg / ml at a molar ratio of 1:1, heat it at 60 degrees for one hour, and then add the perovskite CH 3 NH 3 PbBr 3 The precursor solution is deposited on Au@SiO while r...
Embodiment 3
[0046] The commercial ITO was sonicated in an ultrasonic cleaning machine for 15 minutes each through acetone, detergent, deionized water and isopropanol, then dried with a nitrogen stream, and then treated with ozone for 20 minutes.
[0047] Place the cleaned and ozone-treated ITO glass on a spin coater, spin-coating at a speed of 3000 revolutions per minute to prepare the hole transport layer PEDOT:PSS, and then anneal it on a 150 degree heating stage for 15 minutes.
[0048] Au@SiO 2 The nanoparticles were prepared into an ethanol solution with a concentration of 0.047pM, then sonicated for 5 minutes, fully dispersed, and then spin-coated on the PEDOT:PSS layer at a speed of 3000 rpm, and annealed at 120 degrees for 5 minutes.
[0049] Mix lead chloride, lead iodide and bromomethylamine at a molar ratio of 1:1:1 to a DMF solution with a concentration of 580mg / ml, heat it at 60 degrees for one hour, and then add the perovskite CH 3 NH 3 PbI x Cl 3-x The precursor solution is deposit...
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