Anti-oxidation flux and preparation method thereof

A flux and anti-oxidation technology, applied in welding equipment, welding media, manufacturing tools, etc., can solve the problems of affecting the anti-oxidation effect and easy re-oxidation, so as to shorten the wetting time, prevent excessive oxidation, and reduce tension Effect

Inactive Publication Date: 2016-08-17
傅兴琴
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this patent improves the anti-oxidation performance of the flux by adding antioxidants. During the welding process, the base metal to be welded is easily oxidized again, and the wetting time is too long to affect the anti-oxidation effect.
[0004] The Chinese patent application with the application number CN201610157719.5 discloses a new type of environmentally friendly flux, which includes solvents, surfactants and additives. The main components of the flux include deionized water, polypropylene glycol 1200, and hydroxybenzotriazole , secondary alcohol polyoxyethylene ether, tripropylene glycol butyl ether, tetraethylene glycol dimethyl ether, succinic acid and aliphatic dicarboxylic acid mixture, the solvent of the flux is different types of deionized water, alcohols and ethers Mixed composition, the mixed solvent has a suitable boiling point, more polar groups and medium viscosity, endows the flux with high activity, very little residue, and forms a protective effect on the soldering surface. Different types and components of surfactants are combined Use, has a good synergistic effect, can improve solder wettability, prevent oxidation, although the flux has a certain anti-oxidation performance, but the same, in the welding process, the base metal to be welded is easy to oxidize again, the wetting time Too long will affect the antioxidant effect

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Anti-oxidation flux, including the following raw materials in parts by weight: 150 parts of vegetable oil modified rosin, 130 parts of ethanol, 70 parts of carbitol, 80 parts of polyethylene glycol, 40 parts of sebacic acid, 60 parts of maleic acid , 94 parts of malic acid, 47 parts of citric acid, 25 parts of butyl acetate, 10 parts of amine malonate, 40 parts of nicotinamide, 15 parts of zinc nitrate, 40 parts of glycerol trioleate, 60 parts of isocyanate, difluoro dichloro 70 parts of methane.

[0018] The preparation method of the above-mentioned anti-oxidation flux comprises the following steps: first ethanol, isopropanol, polyethylene glycol, carbitol, sebacic acid, maleic acid, malic acid, citric acid, butyl acetate, Add amine malonate into the reaction kettle, stir and dissolve, then add vegetable oil modified rosin, zinc nitrate, glycerol trioleate, isocyanate, difluorodichloromethane in sequence, after stirring evenly, heat to 80°C for 2 hours, add smoke Amid...

Embodiment 2

[0022] Anti-oxidation flux, including the following raw materials in parts by weight: 100 parts of vegetable oil modified rosin, 120 parts of ethanol, 60 parts of carbitol, 40 parts of polyethylene glycol, 20 parts of sebacic acid, 50 parts of maleic acid , 90 parts of malic acid, 40 parts of citric acid, 20 parts of butyl acetate, 7 parts of amine malonate, 20 parts of nicotinamide, 10 parts of zinc nitrate, 20 parts of glycerol trioleate, 40 parts of isocyanate, difluoro dichloro 40 parts of methane.

[0023] The preparation method of the above-mentioned anti-oxidation flux comprises the following steps: first ethanol, isopropanol, polyethylene glycol, carbitol, sebacic acid, maleic acid, malic acid, citric acid, butyl acetate, Add amine malonate into the reaction kettle, stir and dissolve, add vegetable oil modified rosin, zinc nitrate, glycerol trioleate, isocyanate, difluorodichloromethane in sequence, after stirring evenly, heat to 75°C for 1 hour, add smoke Amide, stir...

Embodiment 3

[0027] Anti-oxidation flux, including the following raw materials in parts by weight: 200 parts of vegetable oil modified rosin, 150 parts of ethanol, 80 parts of carbitol, 120 parts of polyethylene glycol, 60 parts of sebacic acid, and 80 parts of maleic acid , 100 parts of malic acid, 60 parts of citric acid, 30 parts of butyl acetate, 15 parts of amine malonate, 60 parts of nicotinamide, 20 parts of zinc nitrate, 60 parts of glycerol trioleate, 80 parts of isocyanate, difluoro dichloro 90 parts of methane.

[0028] The preparation method of the above-mentioned anti-oxidation flux comprises the following steps: first ethanol, isopropanol, polyethylene glycol, carbitol, sebacic acid, maleic acid, malic acid, citric acid, butyl acetate, Add amine malonate into the reaction kettle, stir and dissolve, then add vegetable oil modified rosin, zinc nitrate, glycerol trioleate, isocyanate, difluorodichloromethane in sequence, after stirring evenly, heat to 85°C for 3 hours, add smoke...

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PUM

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Abstract

The invention discloses an anti-oxidation flux and a preparation method thereof. The anti-oxidation flux is prepared from, by weight, 100-200 parts of vegetable oil modified rosin, 120-150 parts of ethyl alcohol, 60-80 parts of carbitol, 40-120 parts of polyethylene glycol, 20-60 parts of sebacic acid, 50-80 parts of maleic acid, 90-100 parts of malic acid, 40-60 parts of citric acid, 20-30 parts of butyl acetate, 7-15 parts of malonic acid amide, 20-60 parts of nicotinamide, 10-20 parts of zinc nitrate, 20-60 parts of olein, 40-80 parts of isocyanate and 40-90 parts of dichlorodifluoromethane. The preparation method includes: adding the raw materials, performing heating reaction, adding the nicotinamide, and well stirring. The anti-oxidation flux is excellent in wettability, surface tension of welded materials is reduced, and accordingly surface oxidation of the welded materials is prevented.

Description

technical field [0001] The invention relates to an anti-oxidation flux and a preparation method thereof. Background technique [0002] In the atmosphere, the surface of the base metal to be welded is always covered by an oxide film, and its thickness is about 2×10-9~2×10-8m. During welding, the oxide film will inevitably prevent the solder from wetting the base metal, and the welding will not proceed normally. In addition, the base metal needs to be heated during the welding process, and the oxidation of the metal surface will be accelerated at high temperature. Flux is usually a mixture of rosin as the main component, which is an auxiliary material to ensure the smooth progress of the soldering process. Welding is the main process in electronic assembly. Flux is an auxiliary material used in welding. The main function of flux is to remove the oxides on the surface of the solder and the base material to be welded, so that the metal surface can reach the necessary cleanli...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B23K35/363
CPCB23K35/3613B23K35/362
Inventor 傅兴琴
Owner 傅兴琴
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