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Preparation method of doped polarization-maintaining optical fiber

A polarization-maintaining optical fiber and ion technology, applied in the field of optical fiber manufacturing, to achieve the effects of high processing precision, high flatness, and weakened damage

Inactive Publication Date: 2016-11-09
YANSHAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the limitations of the active polarization-maintaining fiber processing technology, no domestic unit has developed an erbium-ytterbium co-doped polarization-maintaining fiber that can meet practical requirements.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A method for preparing a doped polarization-maintaining optical fiber, the specific steps are as follows:

[0021] (1) Add nanoporous silica powder with a particle size of 100nm to the inorganic salt solution of rare earth and co-doped ions. The molar concentration ratio of co-doped ions and rare earth ions in the solution is 10:1, and then the solution is adjusted by ammonia water. When the pH value reaches 7, stir continuously to form a suspension; perform high-speed centrifugation to separate solid particles and liquids, then dry, dehydrate, and granulate to form ion-adsorbed silica particles;

[0022] (2) The ion-adsorbed silica particles are formed by isostatic pressing, and then dehydrated and purified by chlorine gas; then, they are sintered at high temperature for 12 hours in an atmosphere furnace, and the sintering temperature is 1000°C; the surface is processed and chemically cleaned to obtain a cylindrical shape. Rare earth doped silica mandrel;

[0023] (3)...

Embodiment 2

[0029] A method for preparing a doped polarization-maintaining optical fiber, the specific steps are as follows:

[0030] (1) Add nanoporous silica powder with a particle size of 110nm to the rare earth and co-doped ion inorganic salt solution. The molar concentration ratio of co-doped ions and rare earth ions in the solution is 12:1, and then the solution is adjusted by ammonia water. When the pH value reaches 8, stir continuously to form a suspension; perform high-speed centrifugation to separate solid particles and liquids, then dry, dehydrate, and granulate to form ion-adsorbed silica particles;

[0031] (2) The ion-adsorbed silica particles are formed by isostatic pressing, and then dehydrated and purified by chlorine gas; then, they are sintered at high temperature for 13 hours in an atmosphere furnace, and the sintering temperature is 1100°C; the surface is processed and chemically cleaned to obtain a cylindrical shape. Rare earth doped silica mandrel;

[0032] (3) Pla...

Embodiment 3

[0038] A method for preparing a doped polarization-maintaining optical fiber, the specific steps are as follows:

[0039] (1) The nanoporous silica powder with a particle size of 120nm is added to the rare earth and co-doped ion inorganic salt solution, the molar concentration ratio of the co-doped ion and the rare earth ion in the solution is 15:1, and then the solution is adjusted by ammonia water When the pH value reaches 9, stir continuously to form a suspension; perform high-speed centrifugation to separate solid particles and liquids, then dry, dehydrate, and granulate to form ion-adsorbed silica particles;

[0040] (2) The ion-adsorbed silica particles are formed by isostatic pressing, and then dehydrated and purified by chlorine gas; then, they are sintered at high temperature for 14 hours in an atmosphere furnace, and the sintering temperature is 1200°C; the surface is processed and chemically cleaned to obtain a cylindrical shape. Rare earth doped silica mandrel;

[0...

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PUM

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Abstract

The invention discloses a preparation method of a doped polarization-maintaining optical fiber. The method includes the following specific steps of adding nanopore silicon dioxide powder to a rare earth and co-doped ion inorganic salt solution to form a suspension, centrifugally separating solid particles and liquid at high speed, conducting drying, dewatering and granulating to form ion adsorption silicon dioxide particles, conducting isostatic compaction and the like to obtain a cylindrical rare earth doped silicon oxide core bar, conducting drilling, grinding and polishing, and establishing a uniform porous silicon dioxide thin film layer on the inner wall of a core bar tube through a nanometer assembling technology. Silicon dioxide nanometer particles and doping ions are mixed in a solution, the uniformity of the doping ions in the radial direction and the axial direction of the core bar is quite high, the fiber core refraction rate profile has high flatness, the fiber core numerical value aperture precision can be adjusted, the optical fiber has high laser slope efficiency, the stress area of the rare earth ion doped optical fiber prefabricated bar in the ultrasonic drilling process can be effectively reduced by means of a multi-drilling method, and machining precision is high.

Description

technical field [0001] The invention relates to the technical field of optical fiber manufacturing, in particular to a method for preparing a doped polarization-maintaining optical fiber. Background technique [0002] In 1985, researchers at the University of Southampton in the United Kingdom successfully developed rare earth-doped optical fibers using an improved chemical vapor deposition process. In the past 30 years, researchers have continuously improved and innovated the preparation process of rare earth-doped optical fibers, which has led to the continuous and rapid development of rare earth-doped optical fiber amplifiers and lasers. Lasers and their application technology are an important cutting-edge technology in the field of optoelectronics related to national defense and people's livelihood. Compared with other types of lasers such as semiconductor lasers and gas lasers, fiber lasers with rare earth-doped fibers as gain media have high beam quality and high effici...

Claims

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Application Information

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IPC IPC(8): C03B37/012C03B19/06B28D1/14C03C17/23
CPCC03B37/01228B28D1/14C03B19/066C03B2201/34C03B2203/30C03C17/006C03C17/23C03C2217/213C03C2217/425
Inventor 陈月娥李国强邵秋峰王书涛王勇朱艳英贾丽笑
Owner YANSHAN UNIV
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