Preparation method of doped polarization-maintaining optical fiber
A polarization-maintaining optical fiber and ion technology, applied in the field of optical fiber manufacturing, to achieve the effects of high processing precision, high flatness, and weakened damage
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Embodiment 1
[0020] A method for preparing a doped polarization-maintaining optical fiber, the specific steps are as follows:
[0021] (1) Add nanoporous silica powder with a particle size of 100nm to the inorganic salt solution of rare earth and co-doped ions. The molar concentration ratio of co-doped ions and rare earth ions in the solution is 10:1, and then the solution is adjusted by ammonia water. When the pH value reaches 7, stir continuously to form a suspension; perform high-speed centrifugation to separate solid particles and liquids, then dry, dehydrate, and granulate to form ion-adsorbed silica particles;
[0022] (2) The ion-adsorbed silica particles are formed by isostatic pressing, and then dehydrated and purified by chlorine gas; then, they are sintered at high temperature for 12 hours in an atmosphere furnace, and the sintering temperature is 1000°C; the surface is processed and chemically cleaned to obtain a cylindrical shape. Rare earth doped silica mandrel;
[0023] (3)...
Embodiment 2
[0029] A method for preparing a doped polarization-maintaining optical fiber, the specific steps are as follows:
[0030] (1) Add nanoporous silica powder with a particle size of 110nm to the rare earth and co-doped ion inorganic salt solution. The molar concentration ratio of co-doped ions and rare earth ions in the solution is 12:1, and then the solution is adjusted by ammonia water. When the pH value reaches 8, stir continuously to form a suspension; perform high-speed centrifugation to separate solid particles and liquids, then dry, dehydrate, and granulate to form ion-adsorbed silica particles;
[0031] (2) The ion-adsorbed silica particles are formed by isostatic pressing, and then dehydrated and purified by chlorine gas; then, they are sintered at high temperature for 13 hours in an atmosphere furnace, and the sintering temperature is 1100°C; the surface is processed and chemically cleaned to obtain a cylindrical shape. Rare earth doped silica mandrel;
[0032] (3) Pla...
Embodiment 3
[0038] A method for preparing a doped polarization-maintaining optical fiber, the specific steps are as follows:
[0039] (1) The nanoporous silica powder with a particle size of 120nm is added to the rare earth and co-doped ion inorganic salt solution, the molar concentration ratio of the co-doped ion and the rare earth ion in the solution is 15:1, and then the solution is adjusted by ammonia water When the pH value reaches 9, stir continuously to form a suspension; perform high-speed centrifugation to separate solid particles and liquids, then dry, dehydrate, and granulate to form ion-adsorbed silica particles;
[0040] (2) The ion-adsorbed silica particles are formed by isostatic pressing, and then dehydrated and purified by chlorine gas; then, they are sintered at high temperature for 14 hours in an atmosphere furnace, and the sintering temperature is 1200°C; the surface is processed and chemically cleaned to obtain a cylindrical shape. Rare earth doped silica mandrel;
[0...
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